2-methyl-2-nitrosobutane

Base Information

• Chemical Name: 2-methyl-2-nitrosobutane
• CAS No.: 34946-78-6
• Molecular Formula: C5H11NO
• Molecular Weight: 101.1469
• Hs Code.: 2904209090
• Mol file: 34946-78-6.mol

Synonyms:Butane,2-methyl-2-nitroso;2-methyl-2-nitroso-butane;2-Methyl-2-nitroso-butan;

Chemical Property of 2-methyl-2-nitrosobutane

Chemical Property:

• Vapor Pressure: 49mmHg at 25°C
• Melting Point: 50.3-51.2 °C
• Boiling Point: 96.8°C at 760 mmHg
• Flash Point: 20.5°C
• PSA: 29.43000
• Density: 0.86g/cm³
• LogP: 1.94140

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-methyl-2-nitrosobutane

There total 6 articles about 2-methyl-2-nitrosobutane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-methyl-2-butylamine (594-39-8) → 2-methyl-2-nitrosobutane (34946-78-6)

Guidance literature:

With caro's acid;

Reference yield:

N-(1,1-dimethyl-propyl)-hydroxylamine (34495-34-6) → 2-methyl-2-nitrosobutane (34946-78-6)

Guidance literature:

With pyridine; In acetonitrile; (anodic oxidation);

DOI:10.1248/cpb.21.1988

Reference yield:

di-tert-pentyl-diazene dioxide (897918-48-8) → 2-methyl-2-nitrosobutane (34946-78-6)

Guidance literature:

at 13 ℃; Rate constant; Dissoziation in verschiedenen Loesungsmitteln;

DOI:10.1021/ja01573a030

upstream raw materials:

di-tert-pentyl-diazene dioxide

2-methyl-2-butylamine

N-(1,1-dimethyl-propyl)-hydroxylamine

Downstream raw materials:

2-methyl-2-nitrobutane

Refernces

• 1、 Quek, Ser Kiang,Lyapkalo, Ilya M.,Huynh, Han Vinh. "New highly efficient method for the synthesis of tert-alkyl nitroso compounds". . p. 1423 - 1426. Retrieved 2007/10/03.