CID 11730480

Base Information

• Chemical Name: CID 11730480
• CAS No.: 14781-45-4
• Molecular Formula: C10H2 Cu F12 O4
• Molecular Weight: 477.65
• Hs Code.: 29319090
• Mol file: 14781-45-4.mol

Synonyms:

Chemical Property of CID 11730480

Chemical Property:

• Melting Point: 97-99°C
• Boiling Point: 220°C
• Flash Point: 22.8°C
• PSA: 52.60000
• Density: g/cm³
• LogP: 4.08730
• Storage Temp.: Inert atmosphere,Room Temperature
• Sensitive.: moisture sensitive
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 18
• Rotatable Bond Count: 4
• Exact Mass: 476.905744
• Heavy Atom Count: 27
• Complexity: 457

Purity/Quality:

99%, ^*data from raw suppliers

Copper(II)hexafluor-2,4-pentanedionate ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi
• Statements: 20/22-36/37/38
• Safety Statements: 22-36/37-36-26

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

• Canonical SMILES: [CH-](C(=O)C(F)(F)F)C(=O)C(F)(F)F.[CH-](C(=O)C(F)(F)F)C(=O)C(F)(F)F.[Cu+2]

Technology Process of CID 11730480

There total 9 articles about CID 11730480 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

copper(I) oxide + 1,1,1,5,5,5-hexafluoroacetylacetone (1522-22-1) → copper(II) hexafluoroacetylacetonate (14781-45-4)

Guidance literature:

In tetrahydrofuran; for 0.75h; Inert atmosphere;

DOI:10.1016/j.apcata.2017.06.012

Reference yield:

La(β-hexafluoroacetylacetonate)3(H2O)2 complex → copper(II) hexafluoroacetylacetonate (14781-45-4)

Guidance literature:

Multi-step reaction with 2 steps

1: neat (no solvent)

2: chloroform

In chloroform;

Reference yield:

lanthanum tris(hexafluoroacetylacetonate) + Cu(OC(CH3)C(COCH3)NNC6H5)2 → copper(II) hexafluoroacetylacetonate (14781-45-4)

Guidance literature:

In chloroform; La compd. dissolved in min. CHCl3; added slowly to hot soln. of Cu complex in CHCl3; heated for 1 h; cooled; crystd. slowly in air; dried in vac. (60-70°C, 1.33 Pa); detd. byX-ray powder diffraction;

upstream raw materials:

1,1,1,5,5,5-hexafluoroacetylacetone

copper diacetate

Cu(1,1,1,6,6,6-hexafluoropentane-2,4-dionato)2(H₂O)

copper(II) acetate monohydrate

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