7,7,9,9-Tetrachloro-1-oxa-4,6,8,10-tetraza-5lambda5,7lambda5,9lambda5-triphosphaspiro[4.5]deca-5(10),6,8-triene

Base Information

• Chemical Name: 7,7,9,9-Tetrachloro-1-oxa-4,6,8,10-tetraza-5lambda5,7lambda5,9lambda5-triphosphaspiro[4.5]deca-5(10),6,8-triene
• CAS No.: 64487-59-8
• Molecular Formula: C2H5 Cl4 N4 O P3
• Molecular Weight: 335.8206
• NSC Number: 139814
• DSSTox Substance ID: DTXSID30983054

Synonyms:NSC139814;DTXSID30983054;NSC-139814;7,7,9,9-Tetrachloro-1-oxa-4,6,8,10-tetraaza-5lambda~5~,7lambda~5~,9lambda~5~-triphosphaspiro[4.5]deca-5,7,9-triene

Chemical Property of 7,7,9,9-Tetrachloro-1-oxa-4,6,8,10-tetraza-5lambda5,7lambda5,9lambda5-triphosphaspiro[4.5]deca-5(10),6,8-triene

Chemical Property:

• Boiling Point: °Cat760mmHg
• Flash Point: °C
• Density: 2.54g/cm³
• XLogP3: 3.3
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 5
• Rotatable Bond Count: 0
• Exact Mass: 335.840082
• Heavy Atom Count: 14
• Complexity: 388

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1COP2(=NP(=NP(=N2)(Cl)Cl)(Cl)Cl)N1

Technology Process of 7,7,9,9-Tetrachloro-1-oxa-4,6,8,10-tetraza-5lambda5,7lambda5,9lambda5-triphosphaspiro[4.5]deca-5(10),6,8-triene

There total 4 articles about 7,7,9,9-Tetrachloro-1-oxa-4,6,8,10-tetraza-5lambda5,7lambda5,9lambda5-triphosphaspiro[4.5]deca-5(10),6,8-triene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

ethanolamine (141-43-5) → 7,7,9,9-tetrachloro-1-oxa-4,6,8,10-tetraaza-5λ5,7λ5,9λ5-triphospha-spiro[4.5]deca-5,7,9-triene (64487-59-8)

Guidance literature:

With 2,2,4,4,6,6-hexachloro-1,3,5-triaza-2,4,6-triphosphorine; triethylamine; In tetrahydrofuran; for 6h;

DOI:10.1016/S0022-2860(97)00007-0

Reference yield: 66.7%

ethanolamine (141-43-5) → 7,7,9,9-tetrachloro-1-oxa-4,6,8,10-tetraaza-5λ5,7λ5,9λ5-triphospha-spiro[4.5]deca-5,7,9-triene (64487-59-8)

Guidance literature:

In tetrahydrofuran; at 25 ℃; for 6h;

DOI:10.1039/DT9800000840

Reference yield:

2-(trimethylsilyloxy)ethanamine (5804-92-2) → 7,7,9,9-tetrachloro-1-oxa-4,6,8,10-tetraaza-5λ5,7λ5,9λ5-triphospha-spiro[4.5]deca-5,7,9-triene (64487-59-8)

Guidance literature:

With 2,2,4,4,6,6-hexachloro-1,3,5-triaza-2,4,6-triphosphorine;

DOI:10.1080/10426509608545095

upstream raw materials:

ethanolamine

2-(trimethylsilyloxy)ethanamine

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