3,7,12-triformoxycholan-24-al

Base Information

Chemical Name:3,7,12-triformoxycholan-24-al
CAS No.:84965-66-2
Molecular Formula:C27H40O7
Molecular Weight:0
Hs Code.:
Mol file:84965-66-2.mol

Synonyms:3α.7α.12α-triformyloxy-5β-cholanal-(24);Formic acid (3R,5S,7R,8R,9S,10S,12S,13R,14S,17R)-7,12-diformyloxy-10,13-dimethyl-17-((R)-1-methyl-4-oxo-butyl)-hexadecahydro-cyclopenta[a]phenanthren-3-yl ester;3α,7α,12α-triformoxy-5β-cholan-24-al;

Suppliers and Price of 3,7,12-triformoxycholan-24-al

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 3 raw suppliers

Chemical Property of 3,7,12-triformoxycholan-24-al

Chemical Property:

Vapor Pressure:2.26E-12mmHg at 25°C
Melting Point:110 °C (ethanol)
Boiling Point:555.4°C at 760 mmHg
Flash Point:234.5°C
PSA：95.97000
Density:1.16g/cm³
LogP:6.01280

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3,7,12-triformoxycholan-24-al

There total 5 articles about 3,7,12-triformoxycholan-24-al which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 96736-29-7
3α,7α,12α-triformyloxy-5β-24-hydroxy-cholane

: 84965-66-2
3α,7α,12α-triformyloxy-5β-cholan-24-al

Guidance literature:: With sodium acetate; pyridinium chlorochromate; In dichloromethane; for 19h; Ambient temperature;
DOI:10.1016/0039-128X(84)90027-8

Reference yield:

: 2097-89-4
cholic acid triformate

: 84965-66-2
3α,7α,12α-triformyloxy-5β-cholan-24-al

Guidance literature:: Multi-step reaction with 2 steps

1: SOCl₂ / benzene / 2 h / Ambient temperature

2: tetramethylammonium hydridoirontetracarbonyl / CH₂Cl₂ / 4 h / Ambient temperature

With thionyl chloride; tetramethylammonium hydridoirontetracarbonyl; In dichloromethane; benzene;
DOI:10.1016/0039-128X(82)90140-4

Reference yield:

: 74670-08-9
(3α,5β,7α,12α)-3,7,12-tris(formyloxy)cholan-24-oyl chloride

: 84965-66-2
3α,7α,12α-triformyloxy-5β-cholan-24-al

Guidance literature:: With tetramethylammonium hydridoirontetracarbonyl; In dichloromethane; for 4h; Yield given; Ambient temperature;
DOI:10.1016/0039-128X(82)90140-4