4H-(1,2,4)Triazolo(4,3-a)(1,5)benzodiazepin-5-amine, N,N-di-2-propenyl-

Base Information

Chemical Name:4H-(1,2,4)Triazolo(4,3-a)(1,5)benzodiazepin-5-amine, N,N-di-2-propenyl-
CAS No.:137731-10-3
Molecular Formula:C16H17N5
Molecular Weight:279.3397
Hs Code.:
DSSTox Substance ID:DTXSID10160280
Nikkaji Number:J425.852E
Mol file:137731-10-3.mol

Synonyms:BRN 4813890;4H-(1,2,4)Triazolo(4,3-a)(1,5)benzodiazepin-5-amine, N,N-di-2-propenyl-;N,N-Di-2-propenyl-4H-(1,2,4)triazolo(4,3-a)(1,5)benzodiazepin-5-amine;137731-10-3;DTXSID10160280;LS-156297;5-[Bis(2-propenyl)amino]-4H-[1,2,4]triazolo[4,3-a][1,5]benzodiazepine

Suppliers and Price of 4H-(1,2,4)Triazolo(4,3-a)(1,5)benzodiazepin-5-amine, N,N-di-2-propenyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 4H-(1,2,4)Triazolo(4,3-a)(1,5)benzodiazepin-5-amine, N,N-di-2-propenyl-

Chemical Property:

Vapor Pressure:2.62E-09mmHg at 25°C
Boiling Point:478.2°C at 760 mmHg
Flash Point:243°C
Density:1.17g/cm³
XLogP3:1.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:5
Exact Mass:279.14839556
Heavy Atom Count:21
Complexity:409

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C=CCN(CC=C)C1=NC2=CC=CC=C2N3C=NN=C3C1

Technology Process of 4H-(1,2,4)Triazolo(4,3-a)(1,5)benzodiazepin-5-amine, N,N-di-2-propenyl-

There total 2 articles about 4H-(1,2,4)Triazolo(4,3-a)(1,5)benzodiazepin-5-amine, N,N-di-2-propenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 62537-60-4
2-(Dimethylamino)-1,3-dihydro-2H-1,5-benzodiazepin-2-one

: 137731-10-3
Diallyl-(4H-2,3,6,10b-tetraaza-benzo[e]azulen-5-yl)-amine

Guidance literature:: Multi-step reaction with 2 steps

1: 54 percent / glacial CH₃COOH / various solvent(s) / 2 h / 200 °C

2: 1.) titanium tetrachloride, anisole / 1.) toluene, 0 deg C, 2.) toluene, 6h

With titanium tetrachloride; acetic acid; methoxybenzene; In various solvent(s);
DOI:10.1016/0223-5234(91)90144-C

Reference yield:

: 137731-06-7
4H-<1,2,4>-triazolo<4,3-a><1,5>benzodiazepin-5(6H)-one

: 124-02-7
diallylamine

: 137731-10-3
Diallyl-(4H-2,3,6,10b-tetraaza-benzo[e]azulen-5-yl)-amine

Guidance literature:: With titanium tetrachloride; methoxybenzene; Yield given. Multistep reaction; 1.) toluene, 0 deg C, 2.) toluene, 6h;
DOI:10.1016/0223-5234(91)90144-C