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Produce Diallylamine 124-02-7 C6H11N
Cas No: 124-02-7
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124-02-7 Usage

InChI:InChI=1/C6H11N/c1-3-5-7-6-4-2/h3-4,7H,1-2,5-6H2

124-02-7 Well-known Company Product Price

Brand (Code)Product description CAS number Packaging Price Detail
Alfa Aesar (A18950)  Diallylamine, 98%    124-02-7 100ml 221.0CNY Detail
Alfa Aesar (A18950)  Diallylamine, 98%    124-02-7 500ml 461.0CNY Detail

124-02-7SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

Version: 1.0

Creation Date: Aug 10, 2017

Revision Date: Aug 10, 2017

1.Identification

1.1 GHS Product identifier

Product name Diallylamine

1.2 Other means of identification

Product number -
Other names diallyamine

1.3 Recommended use of the chemical and restrictions on use

Identified uses For industry use only. Intermediates
Uses advised against no data available

1.4 Supplier's details

1.5 Emergency phone number

Emergency phone number -
Service hours Monday to Friday, 9am-5pm (Standard time zone: UTC/GMT +8 hours).

More Details:124-02-7 SDS

124-02-7Synthetic route

Diallyl-carbamic acid 1-(3,5-dimethoxy-phenyl)-2-oxo-2-phenyl-ethyl ester

Diallyl-carbamic acid 1-(3,5-dimethoxy-phenyl)-2-oxo-2-phenyl-ethyl ester

A

5,7-Dimethoxy-2-phenylbenzofuran
34911-33-6

5,7-Dimethoxy-2-phenylbenzofuran

B

diallylamine
124-02-7

diallylamine

Conditions
ConditionsYield
In benzene Irradiation;A 96%
B 56%
N,N-Diallylpyridine-2-sulfonamide

N,N-Diallylpyridine-2-sulfonamide

diallylamine
124-02-7

diallylamine

Conditions
ConditionsYield
With samarium diiodide In tetrahydrofuran for 4h; Ambient temperature;90%
N-butylamine
109-73-9

N-butylamine

allyl alcohol
107-18-6

allyl alcohol

A

N-allyl-N-butylamine
4538-09-4

N-allyl-N-butylamine

B

diallylamine
124-02-7

diallylamine

Conditions
ConditionsYield
With ammonium hexafluorophosphate; [Pt(η3-C3H5)(DPP-Xantphos)]PF6 In toluene; acetonitrile at 30℃; for 44h; Inert atmosphere;A 85%
B 4%
hexan-1-amine
111-26-2

hexan-1-amine

allyl alcohol
107-18-6

allyl alcohol

A

N-allylhexan-1-amine
22774-71-6

N-allylhexan-1-amine

B

diallylamine
124-02-7

diallylamine

Conditions
ConditionsYield
With ammonium hexafluorophosphate; [Pt(η3-C3H5)(DPP-Xantphos)]PF6 In toluene; acetonitrile at 50℃; for 8h; Inert atmosphere;A 81%
B 7%
allyl alcohol
107-18-6

allyl alcohol

benzylamine
100-46-9

benzylamine

A

Allylbenzylamine
4383-22-6

Allylbenzylamine

B

diallylamine
124-02-7

diallylamine

Conditions
ConditionsYield
With ammonium hexafluorophosphate; [Pt(η3-C3H5)(DPP-Xantphos)]PF6 In toluene; acetonitrile at 30℃; for 20h; Inert atmosphere;A 80%
B 7%
N,N-diallyl-2-phenyl-2-propen-1-amine

N,N-diallyl-2-phenyl-2-propen-1-amine

tert.-butyl lithium
594-19-4

tert.-butyl lithium

A

(4,4-dimethylpent-1-en-2-yl)benzene
7283-47-8

(4,4-dimethylpent-1-en-2-yl)benzene

B

diallylamine
124-02-7

diallylamine

Conditions
ConditionsYield
Stage #1: N,N-diallyl-2-phenyl-2-propen-1-amine; tert.-butyl lithium In tetrahydrofuran at -78 - 0℃;
Stage #2: With water In tetrahydrofuran
A n/a
B 79%
N,N-diallyltritylamine

N,N-diallyltritylamine

diallylamine
124-02-7

diallylamine

Conditions
ConditionsYield
Stage #1: N,N-diallyltritylamine With naphthalene; lithium In tetrahydrofuran at 0℃; for 6h;
Stage #2: With water In tetrahydrofuran at 0 - 20℃;
62%
Diallylcyanamid
538-08-9

Diallylcyanamid

diallylamine
124-02-7

diallylamine

Conditions
ConditionsYield
With sulfuric acid
With sulfuric acid In water at 30℃;
allyl bromide
106-95-6

allyl bromide

1-amino-2-propene
107-11-9

1-amino-2-propene

diallylamine
124-02-7

diallylamine

1-amino-2-propene
107-11-9

1-amino-2-propene

3-chloroprop-1-ene
107-05-1

3-chloroprop-1-ene

diallylamine
124-02-7

diallylamine

1,2-propanediene
463-49-0

1,2-propanediene

1-amino-2-propene
107-11-9

1-amino-2-propene

A

Triallylamine
102-70-5

Triallylamine

B

N-allyl(2,3-dimethylene)butylamine
86660-16-4

N-allyl(2,3-dimethylene)butylamine

C

Diallyl-(3-methyl-2-methylene-but-3-enyl)-amine
86660-17-5

Diallyl-(3-methyl-2-methylene-but-3-enyl)-amine

D

Allyl-bis-(3-methyl-2-methylene-but-3-enyl)-amine

Allyl-bis-(3-methyl-2-methylene-but-3-enyl)-amine

E

diallylamine
124-02-7

diallylamine

Conditions
ConditionsYield
sodium tetrahydroborate; triphenylphosphine; palladium dichloride at 150℃; for 1h; Product distribution; other temperatures, times; reaction with diallyl amine and N-allyl(2,3-dimethylene)butylamine; telomerization of propadiene with allyl amines;
1,2-propanediene
463-49-0

1,2-propanediene

1-amino-2-propene
107-11-9

1-amino-2-propene

A

N-allyl(2,3-dimethylene)butylamine
86660-16-4

N-allyl(2,3-dimethylene)butylamine

B

Diallyl-(3-methyl-2-methylene-but-3-enyl)-amine
86660-17-5

Diallyl-(3-methyl-2-methylene-but-3-enyl)-amine

C

Allyl-bis-(3-methyl-2-methylene-but-3-enyl)-amine

Allyl-bis-(3-methyl-2-methylene-but-3-enyl)-amine

D

diallylamine
124-02-7

diallylamine

Conditions
ConditionsYield
sodium tetrahydroborate; triphenylphosphine; palladium dichloride at 130℃; for 3h;
1,2-propanediene
463-49-0

1,2-propanediene

A

Diallyl-(3-methyl-2-methylene-but-3-enyl)-amine
86660-17-5

Diallyl-(3-methyl-2-methylene-but-3-enyl)-amine

B

diallylamine
124-02-7

diallylamine

Conditions
ConditionsYield
sodium tetrahydroborate; triphenylphosphine; palladium dichloride at 130℃; for 6h;
(R)-5-Allylaminomethyl-2,7,8-trimethyl-2-((4R,8R)-4,8,12-trimethyl-tridecyl)-chroman-6-ol; hydrobromide

(R)-5-Allylaminomethyl-2,7,8-trimethyl-2-((4R,8R)-4,8,12-trimethyl-tridecyl)-chroman-6-ol; hydrobromide

allylHal

allylHal

diallylamine
124-02-7

diallylamine

Conditions
ConditionsYield
With sodium hydroxide 1.) CH2Cl2, -20 deg C, 10 min, 2.) room temperature, 30 min, 3.) 70 deg C, 1 h; Yield given. Multistep reaction;
ammonia
7664-41-7

ammonia

3-chloroprop-1-ene
107-05-1

3-chloroprop-1-ene

A

Triallylamine
102-70-5

Triallylamine

B

1-amino-2-propene
107-11-9

1-amino-2-propene

C

diallylamine
124-02-7

diallylamine

Conditions
ConditionsYield
at 97 - 105℃; unter Druck;
3-chloroprop-1-ene
107-05-1

3-chloroprop-1-ene

A

diallylamine
124-02-7

diallylamine

B

allylamine and triallylamine

allylamine and triallylamine

Conditions
ConditionsYield
With ammonia at 97 - 105℃; under 5884.06 - 11032.6 Torr;
With ammonia at 97 - 105℃; under 5884.06 - 11032.6 Torr;
ethanol
64-17-5

ethanol

3-chloroprop-1-ene
107-05-1

3-chloroprop-1-ene

A

diallylamine
124-02-7

diallylamine

B

allylamine and triallylamine

allylamine and triallylamine

Conditions
ConditionsYield
With ammonia at 10℃;
Diallylcyanamid
538-08-9

Diallylcyanamid

diluted alkaline solution

diluted alkaline solution

diallylamine
124-02-7

diallylamine

Conditions
ConditionsYield
Hydrolysis;
Diallylcyanamid
538-08-9

Diallylcyanamid

diluted mineral acid

diluted mineral acid

diallylamine
124-02-7

diallylamine

Conditions
ConditionsYield
Hydrolysis;
Triallylamine
102-70-5

Triallylamine

A

diallylamine
124-02-7

diallylamine

B

polymer of acrylaldehyde

polymer of acrylaldehyde

Conditions
ConditionsYield
With alkaline potassium hexacyanoferrate(III) In ethanol at 25℃; Mechanism; Rate constant; Kinetics; variations in the ionic strength of the reaction medium (cations and anions), varying amount of solvent; ΔG(excit.), ΔH(excit.), ΔS(excit.);
benzyl diallylcarbamate
25070-76-2

benzyl diallylcarbamate

diallylamine
124-02-7

diallylamine

Conditions
ConditionsYield
With naphthalen-1-yl-lithium In tetrahydrofuran at 0℃; for 1h;62 % Chromat.
3-chloroprop-1-ene
107-05-1

3-chloroprop-1-ene

A

Triallylamine
102-70-5

Triallylamine

B

1-amino-2-propene
107-11-9

1-amino-2-propene

C

diallylamine
124-02-7

diallylamine

Conditions
ConditionsYield
Stage #1: 3-chloroprop-1-ene With formaldehyd; ammonia In methanol; water at 40 - 70℃; for 6h;
Stage #2: With hydroxyammonium sulfate; sulfuric acid In methanol; water at 40℃; for 0.5h; pH=0.8;
Stage #3: With sodium hydroxide In methanol; water pH=12; Product distribution / selectivity;
Stage #1: 3-chloroprop-1-ene With ammonia In methanol; water at 40 - 70℃; for 6h;
Stage #2: With hydroxyammonium sulfate; sulfuric acid In methanol; water at 40℃; for 0.5h; pH=0.8;
Stage #3: With sodium hydroxide In methanol; water pH=12; Product distribution / selectivity;
With ammonium hydroxide at 35℃; for 0.666667h; Temperature;
piperidine
110-89-4

piperidine

C13H23NO
26256-86-0

C13H23NO

A

1-(piperidin-1-yl)heptan-1-one
18494-53-6

1-(piperidin-1-yl)heptan-1-one

B

diallylamine
124-02-7

diallylamine

Conditions
ConditionsYield
With Al2(NMe2)6 In toluene at 90℃; for 16h; Equilibrium constant;
C13H23NO
26256-86-0

C13H23NO

benzyl-methyl-amine
103-67-3

benzyl-methyl-amine

A

C15H23NO
1002752-21-7

C15H23NO

B

diallylamine
124-02-7

diallylamine

Conditions
ConditionsYield
With Al2(NMe2)6 In toluene at 90℃; for 16h; Equilibrium constant;
1,2-propanediene
463-49-0

1,2-propanediene

A

Triallylamine
102-70-5

Triallylamine

B

1-amino-2-propene
107-11-9

1-amino-2-propene

C

diallylamine
124-02-7

diallylamine

Conditions
ConditionsYield
With AuC27H42N2(1+)*B(C6F5)4(1-)=(AuC27H42N2)(B(C6F5)4); ammonia In benzene-d6 at -60 - 165℃; Inert atmosphere;
With ammonia; AuC27H42N2(1+)*B(C6F5)4(1-)=(AuC27H42N2)(B(C6F5)4) In benzyl methyl ether; benzene-d6 at -60 - 175℃; Conversion of starting material;
1,2-propanediene
463-49-0

1,2-propanediene

A

1-amino-2-propene
107-11-9

1-amino-2-propene

B

diallylamine
124-02-7

diallylamine

Conditions
ConditionsYield
With AuC27H42N2(1+)*B(C6F5)4(1-)=(AuC27H42N2)(B(C6F5)4); ammonia In benzene-d6 at -60 - 175℃; Inert atmosphere;
Triallylamine
102-70-5

Triallylamine

A

acrolein
107-02-8

acrolein

B

diallylamine
124-02-7

diallylamine

Conditions
ConditionsYield
With rhodium(III) 5,10,15,20-tetra(p-sulfonatophenyl)porphyrin; oxygen; trifluoroacetic acid In water at 100℃; under 760.051 Torr; for 2h;
diphenyl diallylphosphoramidate

diphenyl diallylphosphoramidate

diallylamine
124-02-7

diallylamine

Conditions
ConditionsYield
Stage #1: diphenyl diallylphosphoramidate With water; monoammonium para-toluenesulfonate; o-phthalic dicarboxaldehyde In acetonitrile at 90℃; for 24h; Sealed tube;
Stage #2: With sodium hydroxide In water pH=8 - 9; chemoselective reaction;
Cyclopentene oxide
285-67-6

Cyclopentene oxide

diallylamine
124-02-7

diallylamine

trans-2-(diallylamino)cyclopentanol
77924-51-7

trans-2-(diallylamino)cyclopentanol

Conditions
ConditionsYield
In ethanol for 24h; Heating;100%
In ethanol at 95℃; Sealed tube;100%
With triethylaluminum 1.) toluene, CH2Cl2, 25-30 deg C, 30 min, 2.) room temperature; Yield given. Multistep reaction;
C-phenyl-N-methylnitrone
3376-23-6, 7372-59-0, 59862-60-1

C-phenyl-N-methylnitrone

diallylamine
124-02-7

diallylamine

trans-2,3-dimethyl-6-phenyl-5-(prop-2-enyl)-1,2,5-oxadiazinane

trans-2,3-dimethyl-6-phenyl-5-(prop-2-enyl)-1,2,5-oxadiazinane

Conditions
ConditionsYield
In chloroform at 60℃; for 72h;100%
In chloroform at 60℃; for 72h; Cyclization;100%
diallylamine
124-02-7

diallylamine

ethyl trans-3-phenyl-1-oxirane-2-carboxylate
2272-55-1

ethyl trans-3-phenyl-1-oxirane-2-carboxylate

ethyl (2R*,3R*)-3-chloro-2-(diallylamino)-3-phenylpropanoate

ethyl (2R*,3R*)-3-chloro-2-(diallylamino)-3-phenylpropanoate

Conditions
ConditionsYield
Stage #1: diallylamine; ethyl trans-3-phenyl-1-oxirane-2-carboxylate In ethanol for 12h; Ring cleavage; addition; Heating;
Stage #2: With methanesulfonyl chloride; triethylamine In dichloromethane at 0 - 20℃; for 3h; Rearrangement; chlorination;
100%
Cinnamyl acetate
21040-45-9

Cinnamyl acetate

diallylamine
124-02-7

diallylamine

(E)-N,N-diallyl-3-phenylprop-2-en-1-amine
155687-70-0

(E)-N,N-diallyl-3-phenylprop-2-en-1-amine

Conditions
ConditionsYield
bis(η3-allyl-μ-chloropalladium(II)); (1RS,2RS,3SR,4SR)-1,2,3,4-tetrakis((diphenylphosphanyl)methyl)cyclopentane In water at 25℃; for 40h;100%
bis(η3-allyl-μ-chloropalladium(II)); Tedicyp In water at 25℃; for 40h;99%
bicyclo(3.2.0)hept-2-en-6-one
925211-06-9, 925211-07-0

bicyclo(3.2.0)hept-2-en-6-one

5-phenyl-[1,2,4]triazine-3-carboxylic acid ethyl ester
126421-91-8

5-phenyl-[1,2,4]triazine-3-carboxylic acid ethyl ester

diallylamine
124-02-7

diallylamine

[1RS,2RS,3SR,7SR,8SR,11SR,12SR]-9-allyl-12-(ethoxycarbonyl)-14-phenyl-9,13-diazapentacyclo[9.3.1.02,8.03,7.08,12]pentadecadi-4,13-ene

[1RS,2RS,3SR,7SR,8SR,11SR,12SR]-9-allyl-12-(ethoxycarbonyl)-14-phenyl-9,13-diazapentacyclo[9.3.1.02,8.03,7.08,12]pentadecadi-4,13-ene

Conditions
ConditionsYield
With 4 A molecular sieve In chloroform for 21h; Heating;100%
With 4 A molecular sieve In chloroform for 21h; Heating;100%
cyclobutanone
1191-95-3

cyclobutanone

5-phenyl-[1,2,4]triazine-3-carboxylic acid ethyl ester
126421-91-8

5-phenyl-[1,2,4]triazine-3-carboxylic acid ethyl ester

diallylamine
124-02-7

diallylamine

[1RS,2RS,5SR,8SR,9SR]-6-allyl-9-(ethoxycarbonyl)-11-phenyl-6,10-diazatetracyclo[6.2.1.02,5.05,9]dodec-10-ene

[1RS,2RS,5SR,8SR,9SR]-6-allyl-9-(ethoxycarbonyl)-11-phenyl-6,10-diazatetracyclo[6.2.1.02,5.05,9]dodec-10-ene

Conditions
ConditionsYield
With 4 A molecular sieve In chloroform for 22h; Heating;100%
With 4 A molecular sieve In chloroform for 22h; Heating;99%
wortmannin
19545-26-7

wortmannin

diallylamine
124-02-7

diallylamine

acetic acid 4-diallylaminomethylene-6-hydroxy-1α-methoxymethyl-10β,13β-dimethyl-3,7,17-trioxo-1,3,4,7,10,11β,12,13,14α,15,16,17-dodecahydro-2-oxa-cyclopenta[a]phenanthren-11-yl ester

acetic acid 4-diallylaminomethylene-6-hydroxy-1α-methoxymethyl-10β,13β-dimethyl-3,7,17-trioxo-1,3,4,7,10,11β,12,13,14α,15,16,17-dodecahydro-2-oxa-cyclopenta[a]phenanthren-11-yl ester

Conditions
ConditionsYield
In dichloromethane at 20℃; for 1h;100%
In dichloromethane at 20℃; for 1h;68%
diallylamine
124-02-7

diallylamine

(1R,2S,4S)-(+)-(N-bromoacetyl)bornane-10,2-sultam
252577-46-1

(1R,2S,4S)-(+)-(N-bromoacetyl)bornane-10,2-sultam

(1R,2S)-N-[2'-(diallylamino)acetyl]bornane-10,2-sultam
844498-35-7

(1R,2S)-N-[2'-(diallylamino)acetyl]bornane-10,2-sultam

Conditions
ConditionsYield
With potassium carbonate In acetone at 20℃;100%
L-N-Boc-Ala
15761-38-3

L-N-Boc-Ala

diallylamine
124-02-7

diallylamine

(S)-tert-butyl 1-(diallylamino)-1-oxopropan-2-ylcarbamate
950608-92-1

(S)-tert-butyl 1-(diallylamino)-1-oxopropan-2-ylcarbamate

Conditions
ConditionsYield
Stage #1: L-N-Boc-Ala With dicyclohexyl-carbodiimide In dichloromethane at 20℃; for 0.5h; Inert atmosphere;
Stage #2: diallylamine In dichloromethane at 20℃; for 12h; Inert atmosphere;
100%
With dicyclohexyl-carbodiimide In dichloromethane at 20℃; for 12h;
17-formylwortmannin
884540-65-2

17-formylwortmannin

diallylamine
124-02-7

diallylamine

(1E,4S,4aR,5R,6aS,7S)-1-[(diallylamino)methylene]-7-(formyloxy)-11-hydroxy-4-(methoxymethyl)-4a,6a-dimethyl-2,10-dioxo-1,2,4,4a,5,6,6a,7,8,9,9a,10-dodecahydroindeno[4,5-h]isochromen-5-yl acetate

(1E,4S,4aR,5R,6aS,7S)-1-[(diallylamino)methylene]-7-(formyloxy)-11-hydroxy-4-(methoxymethyl)-4a,6a-dimethyl-2,10-dioxo-1,2,4,4a,5,6,6a,7,8,9,9a,10-dodecahydroindeno[4,5-h]isochromen-5-yl acetate

Conditions
ConditionsYield
In dichloromethane for 0.5h;100%
C12H12FNO6
926648-02-4

C12H12FNO6

diallylamine
124-02-7

diallylamine

C18H22N2O6
926648-05-7

C18H22N2O6

Conditions
ConditionsYield
With triethylamine In acetonitrile at 20℃; for 1.5h;100%
diallylamine
124-02-7

diallylamine

Trichloroacetyl chloride
76-02-8

Trichloroacetyl chloride

N,N-diallyl-α,α,α-trichloroacetamide
39089-57-1

N,N-diallyl-α,α,α-trichloroacetamide

Conditions
ConditionsYield
With pyridine In dichloromethane at 0 - 20℃; for 2h;100%
With pyridine In dichloromethane at 20℃; for 2h;94%
2,3-dihydro-2H-furan
1191-99-7

2,3-dihydro-2H-furan

carbon disulfide
75-15-0

carbon disulfide

diallylamine
124-02-7

diallylamine

tetrahydrofuran-2-yl diallylcarbamodithioate
1239488-67-5

tetrahydrofuran-2-yl diallylcarbamodithioate

Conditions
ConditionsYield
In water at 20℃; for 16h; regiospecific reaction;100%
oxalyl dichloride
79-37-8

oxalyl dichloride

Benzoylformic acid
611-73-4

Benzoylformic acid

diallylamine
124-02-7

diallylamine

1-phenyl-2-(diallylamino)ethane-1,2-dione

1-phenyl-2-(diallylamino)ethane-1,2-dione

Conditions
ConditionsYield
Stage #1: oxalyl dichloride; Benzoylformic acid With copper diacetate; N,N-dimethyl-formamide In dichloromethane at 20℃; for 2h;
Stage #2: diallylamine With triethylamine In dichloromethane
100%
N-phenyl-N-methylcarbamoyl chloride
4285-42-1

N-phenyl-N-methylcarbamoyl chloride

diallylamine
124-02-7

diallylamine

1,1-diallyl-3-methyl-3-phenyl-urea

1,1-diallyl-3-methyl-3-phenyl-urea

Conditions
ConditionsYield
With dmap; triethylamine In 1,2-dichloro-ethane Reflux; Inert atmosphere;100%
2-vinylpyridine
100-69-6

2-vinylpyridine

carbon disulfide
75-15-0

carbon disulfide

diallylamine
124-02-7

diallylamine

2-(pyridin-2-yl)ethyl diallylcarbamodithioate

2-(pyridin-2-yl)ethyl diallylcarbamodithioate

Conditions
ConditionsYield
In neat (no solvent) at 20℃; for 6h; Green chemistry; regioselective reaction;100%
Nonanoyl chloride
764-85-2

Nonanoyl chloride

diallylamine
124-02-7

diallylamine

N,N-diallylnonanamide

N,N-diallylnonanamide

Conditions
ConditionsYield
With triethylamine In dichloromethane at 20℃; for 14h; Inert atmosphere;100%
2-bromo-4-methoxybenzenesulfonyl chloride
23095-16-1

2-bromo-4-methoxybenzenesulfonyl chloride

diallylamine
124-02-7

diallylamine

N,N-diallyl-2-bromo-4-methoxybenzenesulfonamide

N,N-diallyl-2-bromo-4-methoxybenzenesulfonamide

Conditions
ConditionsYield
With triethylamine In dichloromethane at 0 - 20℃; for 15h;100%
2-bromo-5-methoxybenzenesulfonyl chloride
179251-57-1

2-bromo-5-methoxybenzenesulfonyl chloride

diallylamine
124-02-7

diallylamine

N,N-diallyl-2-bromo-5-methoxybenzenesulfonamide

N,N-diallyl-2-bromo-5-methoxybenzenesulfonamide

Conditions
ConditionsYield
With triethylamine In dichloromethane at 0 - 20℃; for 15h;100%
phenyl isocyanate
103-71-9

phenyl isocyanate

diallylamine
124-02-7

diallylamine

1,1-diallyl-3-phenylurea
100615-32-5

1,1-diallyl-3-phenylurea

Conditions
ConditionsYield
In diethyl ether at 20℃; for 0.166667h;99%
With 1,6-anhydro-3,4-dideoxy-β-D-glycero-hexopyranos-2-ulose at 0 - 20℃; for 1h;99%
With triethylamine In dichloromethane at 0 - 20℃; for 1h; Inert atmosphere;95%
acryloyl chloride
814-68-6

acryloyl chloride

diallylamine
124-02-7

diallylamine

N,N-diallylacrylamide
3085-68-5

N,N-diallylacrylamide

Conditions
ConditionsYield
With triethylamine In benzene at 0℃; for 0.5h;99%
With trimethylamine In ethyl acetate at 23℃; for 18h; Cooling with ice;75%
With triethylamine In dichloromethane for 24h; Ambient temperature;71%
acrolein
107-02-8

acrolein

diallylamine
124-02-7

diallylamine

3-(N,N-diallylamino)-propanal
142138-16-7

3-(N,N-diallylamino)-propanal

Conditions
ConditionsYield
With 1,8-diazabicyclo[5.4.0]undec-7-ene In tetrahydrofuran at 0℃; Michael addition;99%
With 1,8-diazabicyclo[5.4.0]undec-7-ene In tetrahydrofuran at -15℃; for 0.166667h;95%
With 1,8-diazabicyclo[5.4.0]undec-7-ene In tetrahydrofuran at -15℃; for 0.666667h;
di-tert-butyl dicarbonate
24424-99-5

di-tert-butyl dicarbonate

diallylamine
124-02-7

diallylamine

tert-butyl diallylcarbamate
151259-38-0

tert-butyl diallylcarbamate

Conditions
ConditionsYield
In methanol at 0 - 20℃; for 1h;99%
With iodine at 20℃; for 0.5h;95%
In cyclohexane at 20℃; for 20h;93%
4-chlorobenzoyl chloride
586-75-4

4-chlorobenzoyl chloride

diallylamine
124-02-7

diallylamine

N,N-diallyl-4-bromobenzamide
5866-96-6

N,N-diallyl-4-bromobenzamide

Conditions
ConditionsYield
Stage #1: 4-chlorobenzoyl chloride With pyridine; Merrifield's resin-bound 6-methyl-2-thiouracil In dichloromethane at 80℃; for 0.0833333h; microwave irradiation;
Stage #2: diallylamine In dichloromethane at 80℃; for 0.0833333h; microwave irradiation;
99%
With triethylamine In dichloromethane at 0 - 20℃; for 1h; Inert atmosphere;97%
With triethylamine In dichloromethane at 0 - 20℃;89%
2-bromo-5-methoxy-benzoic acid
22921-68-2

2-bromo-5-methoxy-benzoic acid

diallylamine
124-02-7

diallylamine

N,N-diallyl-2-bromo-5-methoxy-benzamide
851297-49-9

N,N-diallyl-2-bromo-5-methoxy-benzamide

Conditions
ConditionsYield
With dmap; dicyclohexyl-carbodiimide In dichloromethane at 0 - 20℃;99%
furfural
98-01-1

furfural

diallylamine
124-02-7

diallylamine

trans-4,5-bis(diallylamine)cyclopent-2-enone

trans-4,5-bis(diallylamine)cyclopent-2-enone

Conditions
ConditionsYield
With 4C14H11NO3(2-)*2Ni(2+)*2Dy(3+)*2Cl(1-)*2C2H3N In acetonitrile at 20℃; for 24h; Reagent/catalyst; Molecular sieve;99%
In water at 60℃; for 0.0833333h; Microwave irradiation;93%
With 4 A molecular sieve; dysprosium(III) trifluoromethanesulfonate In acetonitrile at 20℃; for 16h;82%
3-chloro-3-oxopropanoic acid methyl ester
37517-81-0

3-chloro-3-oxopropanoic acid methyl ester

diallylamine
124-02-7

diallylamine

methyl 3-(N,N-diallylamino)-3-oxopropanoate
1193366-04-9

methyl 3-(N,N-diallylamino)-3-oxopropanoate

Conditions
ConditionsYield
In dichloromethane at 10 - 20℃;99%
di-tert-butyl dicarbonate
24424-99-5

di-tert-butyl dicarbonate

diallylamine
124-02-7

diallylamine

tert-butyl di(but-3-en-1-yl)carbamate
1211531-07-5

tert-butyl di(but-3-en-1-yl)carbamate

Conditions
ConditionsYield
In methanol at 0 - 20℃;99%
rac-(E)-1,3-diphenyl-3-acetoxy-prop-1-ene
87751-69-7

rac-(E)-1,3-diphenyl-3-acetoxy-prop-1-ene

diallylamine
124-02-7

diallylamine

(S,E)-N,N-diallyl-(1,3-diphenyl-2-propenyl)amine
1202053-74-4

(S,E)-N,N-diallyl-(1,3-diphenyl-2-propenyl)amine

Conditions
ConditionsYield
With C32H31NO2PPd(1+)*F6P(1-); potassium acetate; N,O-bis-(trimethylsilyl)-acetamide at 20℃; for 4h; Inert atmosphere; Neat (no solvent); enantioselective reaction;99%
With N,O-bis-(trimethylsilyl)-acetamide; bis(η3-allyl-μ-chloropalladium(II)); 1-benzyl-5-(((4R,5R)-2-(2-(diphenyl-phosphino)phenyl)-4,5-diphenyl-4,5-dihydro-1H-imidazol-1-yl)methyl)-1H-1,2,3-triazole; potassium acetate In dichloromethane for 24h; Inert atmosphere; Reflux; optical yield given as %ee; enantioselective reaction;
1-ethynyl cobaltocenium hexafluorophosphate
131276-87-4

1-ethynyl cobaltocenium hexafluorophosphate

diallylamine
124-02-7

diallylamine

C18H21CoN(1+)*F6P(1-)

C18H21CoN(1+)*F6P(1-)

Conditions
ConditionsYield
In neat (no solvent) at 35℃; for 1h; Solvent; Time;99%

124-02-7Upstream product

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