2-Benzoyl-1,1-bis(2-chloroethyl)hydrazine

Base Information

• Chemical Name: 2-Benzoyl-1,1-bis(2-chloroethyl)hydrazine
• CAS No.: 33330-30-2
• Molecular Formula: C₁₁H₁₄Cl₂N₂O
• Molecular Weight: 261.151
• NSC Number: 63479
• DSSTox Substance ID: DTXSID10186960
• Nikkaji Number: J73.877H
• Wikidata: Q83058429
• Mol file: 33330-30-2.mol

Synonyms:33330-30-2;2-Benzoyl-1,1-bis(2-chloroethyl)hydrazine;NSC 63479;BRN 2618105;BENZOIC ACID, 2,2-BIS(2-CHLOROETHYL)HYDRAZIDE;1-Benzoyl-2,2-bis(2-chloroethyl)hydrazine;Hydrazine, 2-benzoyl-1,1-bis(2-chloroethyl)-;4-09-00-00923 (Beilstein Handbook Reference);NSC63479;NCIOpen2_002636;DTXSID10186960;Hydrazine,1-bis(2-chloroethyl)-;NSC-63479;N',N'-Bis(2-chloroethyl)benzhydrazide;LS-36172;Benzoic acid,2-bis(2-chloroethyl)hydrazide

Chemical Property of 2-Benzoyl-1,1-bis(2-chloroethyl)hydrazine

Chemical Property:

• PSA: 32.34000
• Density: 1.247g/cm3
• LogP: 2.50190
• XLogP3: 2.6
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 6
• Exact Mass: 260.0483185
• Heavy Atom Count: 16
• Complexity: 202

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C(C=C1)C(=O)NN(CCCl)CCCl

Technology Process of 2-Benzoyl-1,1-bis(2-chloroethyl)hydrazine

There total 5 articles about 2-Benzoyl-1,1-bis(2-chloroethyl)hydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

benzoic acid-[N',N'-bis-(2-hydroxy-ethyl)-hydrazide] (6972-26-5) → benzoic acid-[N',N'-bis-(2-chloro-ethyl)-hydrazide] (33330-30-2)

Guidance literature:

With thionyl chloride; In chloroform;

Reference yield:

benzoic acid hydrazide (613-94-5) → benzoic acid-[N',N'-bis-(2-chloro-ethyl)-hydrazide] (33330-30-2)

Guidance literature:

Multi-step reaction with 2 steps

2: SOCl₂

With thionyl chloride;

Reference yield:

benzoic acid-[N',N'-bis-(2-hydroxy-ethyl)-hydrazide] (6972-26-5) → benzoic acid-[N',N'-bis-(2-chloro-ethyl)-hydrazide] (33330-30-2)

Guidance literature:

With thionyl chloride;

upstream raw materials:

benzoic acid-[N',N'-bis-(2-hydroxy-ethyl)-hydrazide]

1,1-bis(β-chloroethyl)hydrazine hydrochloride

benzoyl chloride

benzoic acid hydrazide

Downstream raw materials:

1,1-bis-(2-chloroethyl)-hydrazine