6-(2-Nitro-4-azidophenylamino)caproate

Base Information

Chemical Name:6-(2-Nitro-4-azidophenylamino)caproate
CAS No.:58775-38-5
Molecular Formula:C₁₂H₁₅N₅O₄
Molecular Weight:293.282
Hs Code.:
DSSTox Substance ID:DTXSID50207502
Wikidata:Q83081417
Mol file:58775-38-5.mol

Synonyms:6-(2-nitro-4-azidophenylamino)caproate;6-(4'-azido-2'-nitrophenylamino)hexanoate;6-ANH;NAZPAC

Suppliers and Price of 6-(2-Nitro-4-azidophenylamino)caproate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 6-(2-Nitro-4-azidophenylamino)caproate

Chemical Property:

Boiling Point:°Cat760mmHg
Flash Point:°C
PSA：144.90000
Density:g/cm³
LogP:3.64246
XLogP3:3.8
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:7
Rotatable Bond Count:8
Exact Mass:293.11240398
Heavy Atom Count:21
Complexity:405

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=C(C=C1N=[N+]=[N-])[N+](=O)[O-])NCCCCCC(=O)O

Technology Process of 6-(2-Nitro-4-azidophenylamino)caproate

There total 1 articles about 6-(2-Nitro-4-azidophenylamino)caproate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 28166-06-5
4-fluoro-3-nitrophenylazide

: 60-32-2,93208-38-9
6-aminohexanoic acid

: 58775-38-5
6-(4-azido-2-nitro-phenylamino)-hexanoic acid

Guidance literature:: With triethylamine; In dimethyl sulfoxide; at 60 ℃;
DOI:10.1016/S0960-894X(00)00009-3

Reference yield:

: 58775-38-5
6-(4-azido-2-nitro-phenylamino)-hexanoic acid

: 6-(4-Azido-2-nitro-phenylamino)-hexanoic acid 2-[(R)-4-hydroxy-2-[2-[(1R,3aS,7aR)-1-((R)-5-hydroxy-1,5-dimethyl-hexyl)-7a-methyl-octahydro-inden-(4E)-ylidene]-eth-(Z)-ylidene]-cyclohex-(E)-ylidene]-ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: DCC; DMAP / CH₂Cl₂

2: TsOH; H₂O / dioxane

With dmap; water; toluene-4-sulfonic acid; dicyclohexyl-carbodiimide; In 1,4-dioxane; dichloromethane; 1: Condensation / 2: Hydroxylation;
DOI:10.1016/S0960-894X(00)00009-3

Reference yield:

: 58775-38-5
6-(4-azido-2-nitro-phenylamino)-hexanoic acid

: 19-methyl[6''-(4-azido-2-nitrophenyl)amino]hexanoyl,25-hydroxy 5E-vitamin D3-3β-(2'-bromoacetate)

Guidance literature:: Multi-step reaction with 3 steps

1: DCC; DMAP / CH₂Cl₂

2: TsOH; H₂O / dioxane

3: DCC; DMAP / CH₂Cl₂

With dmap; water; toluene-4-sulfonic acid; dicyclohexyl-carbodiimide; In 1,4-dioxane; dichloromethane; 1: Condensation / 2: Hydroxylation / 3: Acetylation;
DOI:10.1016/S0960-894X(00)00009-3