1,1,3,3-Tetrachloroacetone

Base Information Edit

Chemical Name:1,1,3,3-Tetrachloroacetone
CAS No.:632-21-3
Molecular Formula:C3H2 Cl4 O
Molecular Weight:195.86
Hs Code.:
European Community (EC) Number:211-172-3
NSC Number:137844
UNII:J7R42FF17P
DSSTox Substance ID:DTXSID1021663
Nikkaji Number:J1.711F
Wikidata:Q27281319
Mol file:632-21-3.mol

Synonyms:1,1,3,3-tetrachloroacetone

Suppliers and Price of 1,1,3,3-Tetrachloroacetone

Supply Marketing:Edit

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
1,1,3,3-Tetrachloroacetone(~85%)
250mg
$ 180.00

Medical Isotopes, Inc.
1,1,3,3-Tetrachloroacetone
2.5 g
$ 2200.00

Total 0 raw suppliers

Chemical Property of 1,1,3,3-Tetrachloroacetone Edit

Chemical Property:

Vapor Pressure:0.527mmHg at 25°C
Melting Point:48-49(水合物)oC
Refractive Index:1.4944 (estimate)
Boiling Point:191°C at 760 mmHg
Flash Point:73.7°C
PSA：17.07000
Density:1.612g/cm³
LogP:2.16290
Storage Temp.:Hygroscopic, -20°C Freezer, Under Inert Atmosphere
Solubility.:Chloroform (Sparingly), Ethyl Acetate (Slightly)
XLogP3:2.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:195.883025
Heavy Atom Count:8
Complexity:79.3

Purity/Quality:: 1,1,3,3-Tetrachloroacetone(~85%) ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C(C(=O)C(Cl)Cl)(Cl)Cl
Uses 1,1,3,3-Tetrachloroacetone is an polychlorinated compound found to be a potent mutagen.

Technology Process of 1,1,3,3-Tetrachloroacetone

There total 24 articles about 1,1,3,3-Tetrachloroacetone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 542-05-2
acetonedicarboxylic acid

: 632-21-3
1,1,3,3-tetrachloropropanone

Guidance literature:: acetonedicarboxylic acid; With sulfuryl dichloride; In diethyl ether; dichloromethane; at -10 - 20 ℃;

Heating;
DOI:10.1080/00304940409355973

Reference yield: 72.0%

: 921-03-9
1,1,3-trichloroacetone

: 632-21-3
1,1,3,3-tetrachloropropanone

: 1768-31-6
pentachloroacetone

Guidance literature:: With sulfuryl dichloride; N-benzyl-N,N,N-triethylammonium chloride; at 55 ℃; for 168h;
DOI:10.1080/00304940409355973

Reference yield: 70.0%

: 78950-58-0
tetrachloroacetone hydrate

: 632-21-3
1,1,3,3-tetrachloropropanone

Guidance literature:: In water; Heating; flash evaporation of water, final azeotropic distillation with hexane.;
DOI:10.1016/S0040-4039(01)93284-8