1-Butanone,3,3'-[(2-hydroxy-1,3-propanediyl)dinitrilo]bis[1-phenyl- (9CI)

Base Information

Chemical Name:1-Butanone,3,3'-[(2-hydroxy-1,3-propanediyl)dinitrilo]bis[1-phenyl- (9CI)
CAS No.:16087-33-5
Molecular Formula:C₂₃H₂₆N₂O₃
Molecular Weight:378.471
Hs Code.:

Synonyms:Butyrophenone,3,3''-[(2-hydroxytrimethylene)dinitrilo]di- (6CI,8CI); NSC 311964

Suppliers and Price of 1-Butanone,3,3'-[(2-hydroxy-1,3-propanediyl)dinitrilo]bis[1-phenyl- (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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Total 5 raw suppliers

Chemical Property of 1-Butanone,3,3'-[(2-hydroxy-1,3-propanediyl)dinitrilo]bis[1-phenyl- (9CI)

Chemical Property:

Boiling Point:566.2°Cat760mmHg
Flash Point:296.2°C
Density:1.09g/cm³

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1-Butanone,3,3'-[(2-hydroxy-1,3-propanediyl)dinitrilo]bis[1-phenyl- (9CI)

There total 1 articles about 1-Butanone,3,3'-[(2-hydroxy-1,3-propanediyl)dinitrilo]bis[1-phenyl- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 616-29-5
1,3-Diamino-2-hydroxypropane

: 93-91-4
1-phenylbutan-1,3-dione

: 16087-33-5
3-{(E)-2-Hydroxy-3-[1-methyl-3-oxo-3-phenyl-prop-(E)-ylideneamino]-propylimino}-1-phenyl-butan-1-one

Guidance literature:: In ethanol; for 2h; Heating;
DOI:10.1039/DT9860002633

Reference yield:

: copper(II) perchlorate hexahydrate

: 16087-33-5
3-{(E)-2-Hydroxy-3-[1-methyl-3-oxo-3-phenyl-prop-(E)-ylideneamino]-propylimino}-1-phenyl-butan-1-one

: Cu₂((C₆H₅COCHCCH₃NCH₂)2CHO)N₃

Guidance literature:: With sodium azide; sodium hydroxide; In ethanol; successively addn. of Cu-compd./NaN3 and NaOH to ethanolic soln. of Schiff base, stirring at room temp. several hours; cooling, recrystn (CHCl3); elem. anal.;
DOI:10.1246/bcsj.67.260

Reference yield:

: 288-13-1
NH-pyrazole

: copper(II) perchlorate hexahydrate

: 16087-33-5
3-{(E)-2-Hydroxy-3-[1-methyl-3-oxo-3-phenyl-prop-(E)-ylideneamino]-propylimino}-1-phenyl-butan-1-one

: Cu₂((C₆H₅COCHCCH₃NCH₂)2CHO)C₃H₃N₂*0.5H₂O

Guidance literature:: With sodium hydroxide; H₂O; In ethanol; addn. of Cu-compd./pyrazole and NaOH to ethanolic soln. of Schiff base, stirring at room temp. several hours; filtration, washing (EtOH, CH2Cl2, acetone); elem. anal.;
DOI:10.1246/bcsj.67.260