(3,4,4-trimethyldioxetan-3-yl)methyl N-chlorosulfonylcarbamate

Base Information

Chemical Name:(3,4,4-trimethyldioxetan-3-yl)methyl N-chlorosulfonylcarbamate
CAS No.:108536-12-5
Molecular Formula:C7H12ClNO6S
Molecular Weight:
Hs Code.:
Mol file:108536-12-5.mol

Synonyms:(3,4,4-trimethyldioxetan-3-yl)methyl N-chlorosulfonylcarbamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3,4,4-trimethyldioxetan-3-yl)methyl N-chlorosulfonylcarbamate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of (3,4,4-trimethyldioxetan-3-yl)methyl N-chlorosulfonylcarbamate

There total 2 articles about (3,4,4-trimethyldioxetan-3-yl)methyl N-chlorosulfonylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 1189-71-5
isocyanate de chlorosulfonyle

: 84114-76-1
3-(Hydroxymethyl)-3,4,4-trimethyl-1,2-dioxetane

: 108536-12-5,109123-65-1
3-<<(chlorosulfonyl)carbamoyloxy>methyl>-3,4,4-trimethyl-1,2-dioxetane

Guidance literature:: In diethyl ether; for 0.5h;
DOI:10.1021/jo00390a018

Reference yield:

: 108536-15-8
2,3-dimethyl-1,2-epoxy-3-hydroperoxybutane

: 108536-12-5,109123-65-1
3-<<(chlorosulfonyl)carbamoyloxy>methyl>-3,4,4-trimethyl-1,2-dioxetane

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / KOH / CH₂Cl₂; H₂O / 5.5 h / 0 °C

2: 76 percent / diethyl ether / 0.5 h

With potassium hydroxide; In diethyl ether; dichloromethane; water;
DOI:10.1021/jo00390a018