2,7-Dinitroanthraquinone

Base Information

• Chemical Name: 2,7-Dinitroanthraquinone
• CAS No.: 605-28-7
• Molecular Formula: C14H6 N2 O6
• Molecular Weight: 298.211
• European Community (EC) Number: 210-084-2
• DSSTox Substance ID: DTXSID00209233
• Nikkaji Number: J134.827B
• Wikidata: Q83083446
• ChEMBL ID: CHEMBL493255
• Mol file: 605-28-7.mol

Synonyms:2,7-Dinitroanthraquinone;605-28-7;EINECS 210-084-2;2,7-Dinitroantraquinone;2,7-dinitroanthracene-9,10-dione;2,7- Dinitroanthrachinon;D07DAX;Anthraquinone, 2,7-dinitro-;CHEMBL493255;SCHEMBL2772220;DTXSID00209233;MFCD00032964;9,10-Anthracenedione, 2,7-dinitro-;SY254122

Chemical Property of 2,7-Dinitroanthraquinone

Chemical Property:

• Vapor Pressure: 1.02E-12mmHg at 25°C
• Melting Point: 239-240 °C
• Boiling Point: 563.4°C at 760 mmHg
• Flash Point: 294°C
• PSA: 125.78000
• Density: 1.631g/cm³
• LogP: 3.32480
• XLogP3: 2.5
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 6
• Rotatable Bond Count: 0
• Exact Mass: 298.02258592
• Heavy Atom Count: 22
• Complexity: 492

Purity/Quality:

98%min ^*data from raw suppliers

2,7-Dinitroanthraquinone ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC2=C(C=C1[N+](=O)[O-])C(=O)C3=C(C2=O)C=CC(=C3)[N+](=O)[O-]

Technology Process of 2,7-Dinitroanthraquinone

There total 13 articles about 2,7-Dinitroanthraquinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

anthracen-9(10H)-one (90-44-8) → 2,7-dinitroanthracene-9,10-dione (605-28-7)

Guidance literature:

anthracen-9(10H)-one; With nitric acid; at 0 - 20 ℃;

With acetic acid; for 3h; Reflux;

DOI:10.1039/c2cc31770b

Reference yield:

→ 2,7-dinitroanthracene-9,10-dione (605-28-7)

Guidance literature:

With chromium(VI) oxide; acetic acid;

Reference yield:

anthracene (120-12-7) → 2,7-dinitroanthracene-9,10-dione (605-28-7)

Guidance literature:

With nitric acid; acetic acid;

upstream raw materials:

anthracene

anthracen-9(10H)-one

9,10-phenanthrenequinone

nitric acid

Downstream raw materials:

2,7-dibromo-9,10-anthraquinone

2,7-dihydroxy-anthraquinone

2,7-diaminoanthraquinone

Refernces

• 1、 -. "Near-infrared carbon rhodamine fluorescent dye and synthetic method thereof". Paragraph 0014; 0015. . Retrieved 2018/12/14.
• 2、 Domasevitch, Konstantin V.,Solntsev, Pavlo V.,Krautscheid, Harald,Zhylenko, Iryna S.,Rusanov, Eduard B.,Chernega, Alexander N.. "Facile access to a series of large polycondensed pyridazines and their utility for the supramolecular synthesis of coordination polymers". supporting information; experimental part. p. 5847 - 5849. Retrieved 2012/07/27.