3,6-Diethyl-1,4-dioxane-2,5-dione

Base Information

• Chemical Name: 3,6-Diethyl-1,4-dioxane-2,5-dione
• CAS No.: 4374-57-6
• Molecular Formula: C8H12O4
• Molecular Weight: 172.181
• Hs Code.: 2934999090
• Mol file: 4374-57-6.mol

Synonyms:1,4-Diketo-2,5-diethyldioxan;3,6-Diaethyl-[1,4]dioxan-2,5-dion;3,6-diethyl-1,4-dioxan-2,5-dione;3,6-diethyl-[1,4]dioxane-2,5-dione;Butanoic acid,bimol. cyclic ester;p-Dioxane-2,3,6-diethyl;1,5-dione,3,6-diethyl;

Chemical Property of 3,6-Diethyl-1,4-dioxane-2,5-dione

Chemical Property:

• Vapor Pressure: 0.000753mmHg at 25°C
• Boiling Point: 306.8°C at 760 mmHg
• Flash Point: 157.2°C
• PSA: 52.60000
• Density: 1.098g/cm³
• LogP: 0.64360

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3,6-Diethyl-1,4-dioxane-2,5-dione

There total 4 articles about 3,6-Diethyl-1,4-dioxane-2,5-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ 3,6-diethyl-1,4-dioxane-2,5-dione (4374-57-6) + (E)-but-2-enoic acid (107-93-7)

Guidance literature:

bei der Destillation im Vakuum;

Reference yield:

2-Hydroxybutanoic acid (600-15-7,565-70-8) → 3,6-diethyl-1,4-dioxane-2,5-dione (4374-57-6)

Guidance literature:

With H-BEA; In o-xylene; for 3h; Dean-Stark; Heating;

Reference yield:

2-Hydroxybutanoic acid (600-15-7,565-70-8) → 3,6-diethyl-1,4-dioxane-2,5-dione (4374-57-6) + C10H24O3Si2 (55133-93-2) + C14H30O5Si2 + C18H36O7Si2

Guidance literature:

With trimethylsilylating agent; Product distribution; multistep reaction: 1.) 125 deg C, 6 h, 2.) trimethylsilylation; further temperature, time effect;

upstream raw materials:

2-Hydroxybutanoic acid

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