3,4'-Dinitrobiphenyl

Base Information

Chemical Name:3,4'-Dinitrobiphenyl
CAS No.:6311-43-9
Molecular Formula:C12H8 N2 O4
Molecular Weight:244.207
Hs Code.:2904209090
European Community (EC) Number:661-655-1
NSC Number:43204
UNII:J1209AC0XE
DSSTox Substance ID:DTXSID40212448
Nikkaji Number:J5.169A
Wikidata:Q83087579
ChEMBL ID:CHEMBL350509
Mol file:6311-43-9.mol

Synonyms:3,4'-Dinitrobiphenyl;1,1'-Biphenyl, 3,4'-dinitro-;6311-43-9;3,4'-Dinitro-1,1'-biphenyl;BIPHENYL, 3,4'-DINITRO-;NSC 43204;BRN 1982974;J1209AC0XE;NSC-43204;1,1'-Biphenyl, 3,4'-dinitro- (9CI);NSC43204;3,4'-Dinitro-biphenyl;1, 3,4'-dinitro-;UNII-J1209AC0XE;CHEMBL350509;SCHEMBL4516641;DTXSID40212448;AKOS024339104;LS-44337

Suppliers and Price of 3,4'-Dinitrobiphenyl

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Sigma-Aldrich
3,4'-DINITROBIPHENYL Aldrich
1ea
$ 144.00

Total 6 raw suppliers

Chemical Property of 3,4'-Dinitrobiphenyl

Chemical Property:

Boiling Point:417oC at 760 mmHg
Flash Point:208.1oC
PSA：91.64000
Density:1.368g/cm3
LogP:4.21640
XLogP3:3.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:1
Exact Mass:244.04840674
Heavy Atom Count:18
Complexity:315

Purity/Quality:

99% ^*data from raw suppliers

3,4'-DINITROBIPHENYL Aldrich ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=CC(=C1)[N+](=O)[O-])C2=CC=C(C=C2)[N+](=O)[O-]

Technology Process of 3,4'-Dinitrobiphenyl

There total 4 articles about 3,4'-Dinitrobiphenyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 4482-01-3
o-benzenedisulfonimide

: 13331-27-6
m-nitrobenzene boronic acid

: 100-01-6,104810-17-5
4-nitro-aniline

: 6311-43-9
3,4'-dinitro-1,1'-biphenyl

Guidance literature:: o-benzenedisulfonimide; 4-nitro-aniline; With acetic acid; at 0 - 5 ℃; for 0.166667h; Inert atmosphere;

With isopentyl nitrite; for 0.166667h; Inert atmosphere;

m-nitrobenzene boronic acid; With bis[(trifluoromethanesulfonyl)imidate]-2-(dicyclohexyl(2’,6’-dimethoxybiphenyl))phosphine gold(I); caesium carbonate; In tetrahydrofuran; at 20 ℃; for 3.5h; chemoselective reaction; Inert atmosphere;
DOI:10.1016/j.tet.2018.08.018

Reference yield: 58.0%

: 13331-27-6
m-nitrobenzene boronic acid

: 100-00-5
4-chlorobenzonitrile

: 6311-43-9
3,4'-dinitro-1,1'-biphenyl

Guidance literature:: With PdCl₂(PPh₃O)2; potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 36h;
DOI:10.1016/j.tetlet.2010.01.032

Reference yield:

: 456-27-9
4-nitrobenzenediazonium tetrafluoroborate

: 98-95-3,26969-40-4
nitrobenzene

: 1528-74-1
4,4'-dinitrobiphenyl

: 6311-43-9
3,4'-dinitro-1,1'-biphenyl

: 606-81-5
2,4'-dinitrobiphenyl

Guidance literature:: In N,N-dimethyl-formamide; at 60 ℃; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
DOI:10.1016/S0040-4020(97)00343-8