7-chloro-2-[(1E)-3,3-dimethyltriaz-1-en-1-yl]-10-methyl-10H-phenothiazine

Base Information

Chemical Name:7-chloro-2-[(1E)-3,3-dimethyltriaz-1-en-1-yl]-10-methyl-10H-phenothiazine
CAS No.:79226-51-0
Molecular Formula:C₁₅H₁₅ClN₄S
Molecular Weight:318.83
Hs Code.:

Synonyms:

Suppliers and Price of 7-chloro-2-[(1E)-3,3-dimethyltriaz-1-en-1-yl]-10-methyl-10H-phenothiazine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 2 raw suppliers

Chemical Property of 7-chloro-2-[(1E)-3,3-dimethyltriaz-1-en-1-yl]-10-methyl-10H-phenothiazine

Chemical Property:

Vapor Pressure:3E-09mmHg at 25°C
Boiling Point:476.7°C at 760 mmHg
Flash Point:242.1°C
Density:1.32g/cm³

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 7-chloro-2-[(1E)-3,3-dimethyltriaz-1-en-1-yl]-10-methyl-10H-phenothiazine

There total 7 articles about 7-chloro-2-[(1E)-3,3-dimethyltriaz-1-en-1-yl]-10-methyl-10H-phenothiazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 95-24-9
6-chloro-2-aminobenzothiazole

: 79226-51-0
C₁₅H₁₅ClN₄S

Guidance literature:: Multi-step reaction with 6 steps

1: 93 percent / ethanol / 15 h / Heating

2: 50percent aq. KOH / Heating

3: 78 percent / sodium carbonate / ethanol / 10 h / Heating

4: 90 percent / copper powder, cuprous iodide, sodium carbonate / dimethylformamide / 12 h / Heating

5: stannous chloride, acetic anhydride, HCl (g) / acetic acid / Ambient temperature

6: 1. sodium nitrite / 1. 48percent fluoroboric acid, -5 degC, 1h; 2. ice cold, 1h; 3. 30 min.

With hydrogenchloride; potassium hydroxide; copper(l) iodide; acetic anhydride; copper; sodium carbonate; tin(ll) chloride; sodium nitrite; In ethanol; acetic acid; N,N-dimethyl-formamide;
DOI:10.1002/jhet.5570180425

Reference yield:

: 79226-37-2
5-chloro-2-methylamino-benzenethiol

: 79226-51-0
C₁₅H₁₅ClN₄S

Guidance literature:: Multi-step reaction with 4 steps

1: 78 percent / sodium carbonate / ethanol / 10 h / Heating

2: 90 percent / copper powder, cuprous iodide, sodium carbonate / dimethylformamide / 12 h / Heating

3: stannous chloride, acetic anhydride, HCl (g) / acetic acid / Ambient temperature

4: 1. sodium nitrite / 1. 48percent fluoroboric acid, -5 degC, 1h; 2. ice cold, 1h; 3. 30 min.

With hydrogenchloride; copper(l) iodide; acetic anhydride; copper; sodium carbonate; tin(ll) chloride; sodium nitrite; In ethanol; acetic acid; N,N-dimethyl-formamide;
DOI:10.1002/jhet.5570180425

Reference yield:

: 79226-43-0
7-Chloro-10-methyl-2-nitro-10H-phenothiazine

: 79226-51-0
C₁₅H₁₅ClN₄S

Guidance literature:: Multi-step reaction with 2 steps

1: stannous chloride, acetic anhydride, HCl (g) / acetic acid / Ambient temperature

2: 1. sodium nitrite / 1. 48percent fluoroboric acid, -5 degC, 1h; 2. ice cold, 1h; 3. 30 min.

With hydrogenchloride; acetic anhydride; tin(ll) chloride; sodium nitrite; In acetic acid;
DOI:10.1002/jhet.5570180425