2-(2,3-Dichlorophenyl)ethanol

Base Information

• Chemical Name: 2-(2,3-Dichlorophenyl)ethanol
• CAS No.: 114686-85-0
• Molecular Formula: C8H8Cl2O
• Molecular Weight: 191.057
• Hs Code.: 2906299090
• DSSTox Substance ID: DTXSID30370485
• Nikkaji Number: J3.641.725K
• Wikidata: Q82157641
• Mol file: 114686-85-0.mol

Synonyms:2-(2,3-dichlorophenyl)ethanol;114686-85-0;2,3-DICHLOROPHENETHYLALCOHOL;2,3-DICHLOROPHENETHYL ALCOHOL;2-(2,3-dichlorophenyl)ethan-1-ol;Benzeneethanol, 2,3-dichloro-;SCHEMBL2963562;DTXSID30370485;FJJDHDLMGJKZKV-UHFFFAOYSA-N;CL8843;MFCD04112742;AKOS012084728;AM82965;DS-1840;2,3-dichlorophenethylalcohol, AldrichCPR;CS-0157237;FT-0691193;J3.641.725K;EN300-1250750;A894158

Chemical Property of 2-(2,3-Dichlorophenyl)ethanol

Chemical Property:

• Vapor Pressure: 0.00196mmHg at 25°C
• Refractive Index: 1.569
• Boiling Point: 279.1 °C at 760 mmHg
• PKA: 14.60±0.10(Predicted)
• Flash Point: 117.9 °C
• PSA: 20.23000
• Density: 1.329 g/cm³
• LogP: 2.52820
• Storage Temp.: Sealed in dry,Room Temperature
• XLogP3: 2.8
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 2
• Exact Mass: 189.9952203
• Heavy Atom Count: 11
• Complexity: 119

Purity/Quality:

97% ^*data from raw suppliers

2-(2,3-Dichlorophenyl)ethanol ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xn
• Hazard Codes: Xn
• Statements: 22-41
• Safety Statements: 24/25

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC(=C(C(=C1)Cl)Cl)CCO

Technology Process of 2-(2,3-Dichlorophenyl)ethanol

There total 1 articles about 2-(2,3-Dichlorophenyl)ethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

C14H22Cl2OSi → 2-(2,3-dichlorophenyl)ethan-1-ol (114686-85-0)

Guidance literature:

With toluene-4-sulfonic acid; In methanol; dichloromethane; at 20 - 25 ℃; for 0.333333h; Flow reactor;

DOI:10.1016/j.tetlet.2017.05.008

Reference yield: 100.0%

2-(2,3-dichlorophenyl)ethan-1-ol (114686-85-0) → 2-(2,3-Dichlorophenyl)ethyl methansulfonate

Guidance literature:

Reference yield: 93.0%

2-(2,3-dichlorophenyl)ethan-1-ol (114686-85-0) + tert-butyldimethylsilyl chloride (18162-48-6) → C14H22Cl2OSi

Guidance literature:

2-(2,3-dichlorophenyl)ethan-1-ol; With 1H-imidazole; In dichloromethane; for 0.0833333h;

tert-butyldimethylsilyl chloride; In dichloromethane; at 20 ℃; for 1h;

DOI:10.1016/j.tetlet.2017.05.008

Downstream raw materials:

2,3-dichlorobenzeneacetaldehyde

1-(2-bromoethyl)-2,3-dichlorobenzene