Acetic acid,2-(diphenylphosphinyl)-, 2-[2-(diphenylphosphinyl)acetyl]hydrazide

Base Information

Chemical Name:Acetic acid,2-(diphenylphosphinyl)-, 2-[2-(diphenylphosphinyl)acetyl]hydrazide
CAS No.:16543-20-7
Molecular Formula:C₂₈H₂₆N₂O₄P₂
Molecular Weight:516.473
Hs Code.:
Mol file:16543-20-7.mol

Synonyms:Aceticacid, (diphenylphosphinyl)-, 2-[(diphenylphosphinyl)acetyl]hydrazide (9CI);Hydrazine, 1,2-bis[(diphenylphosphinyl)acetyl]- (8CI);Bis(diphenylphosphinylacetic acid) hydrazide

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Chemical Property of Acetic acid,2-(diphenylphosphinyl)-, 2-[2-(diphenylphosphinyl)acetyl]hydrazide

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:: SDS file from LookChem

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Technology Process of Acetic acid,2-(diphenylphosphinyl)-, 2-[2-(diphenylphosphinyl)acetyl]hydrazide

There total 4 articles about Acetic acid,2-(diphenylphosphinyl)-, 2-[2-(diphenylphosphinyl)acetyl]hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 16543-10-5
(diphenylphosphoryl)acetic acid hydrazide

: 6361-05-3
ethyl 2-(diphenylphosphoryl)acetate

: 16543-20-7
N,N'-bis-(diphenylphosphinoylacetyl)hydrazine

Guidance literature:: at 120 - 140 ℃; for 1h;

Reference yield: 46.0%

: 121714-78-1,24290-40-2,58694-80-7,10025-77-1,64333-00-2
iron(III) chloride hexahydrate

: 16543-10-5
(diphenylphosphoryl)acetic acid hydrazide

: [(C₆H₅)2POCH₂CONH]2*FeCl₃

: 16543-20-7
N,N'-bis-(diphenylphosphinoylacetyl)hydrazine

Guidance literature:: In ethanol; byproducts: N2, FeCl2, HCl; FeCl3*6H2O added to a soln. of the hydrazide, kept for 0.5 h after reaction was complete; solvent removed in vacuo, filtered off, washed (water), dried in air, org. compound isolated from the mother liquor; elem. anal.;