Tetrahexylammonium iodide

Base Information

• Chemical Name: Tetrahexylammonium iodide
• CAS No.: 2138-24-1
• Molecular Formula: C24H52IN
• Molecular Weight: 481.588
• Hs Code.: 29239000
• European Community (EC) Number: 218-382-4
• NSC Number: 56442
• DSSTox Substance ID: DTXSID50883800
• Mol file: 2138-24-1.mol

Synonyms:tetrahexylammonium;tetrahexylammonium benzoate;tetrahexylammonium bromide;tetrahexylammonium chloride;tetrahexylammonium hydroxide;tetrahexylammonium iodide;tetrahexylammonium perchlorate;tetrahexylammonium sulfate (1:1);tetrahexylammonium thicyanate

Chemical Property of Tetrahexylammonium iodide

Chemical Property:

• Appearance/Colour: beige fluffy powder
• Melting Point: 99-101 °C
• PSA: 0.00000
• Density: 1.0444 (estimate)
• LogP: 5.12840
• Storage Temp.: Keep in dark place,Inert atmosphere,Room temperature
• Sensitive.: Hygroscopic
• Solubility.: almost transparency in Methanol
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 20
• Exact Mass: 481.31445
• Heavy Atom Count: 26
• Complexity: 195

Purity/Quality:

98%,99%, ^*data from raw suppliers

Tetra-n-hexylammonium iodide ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi
• Statements: 36/37/38
• Safety Statements: 26-36

MSDS Files:

SDS file from LookChem

Useful:

• Chemical Classes: Nitrogen Compounds -> Quaternary Amines
• Canonical SMILES: CCCCCC[N+](CCCCCC)(CCCCCC)CCCCCC.[I-]

Technology Process of Tetrahexylammonium iodide

There total 2 articles about Tetrahexylammonium iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

tri-n-hexylamine (102-86-3) + 1-Iodohexane (638-45-9) → tetrahexylammonium iodide (2138-24-1)

Guidance literature:

at 90 ℃; for 18h;

DOI:10.1134/S1070427206030153

Reference yield:

hexan-1-amine (111-26-2) + 1-Iodohexane (638-45-9) → tetrahexylammonium iodide (2138-24-1)

Guidance literature:

In ethanol;

DOI:10.1021/jo01075a616

Reference yield: 32.0%

(2-(((4-(1,3-Dihydro-1-oxo-2H-isoindol-2-yl)butyl)-hydroxyphosphinyl)methyl)-4-phenylbutanoyl)-L-leucine N-phenylamide + ? molecular sieves + propanoic acid,1-chloro-2-methylpropyl ester (58304-65-7) + tetrahexylammonium iodide (2138-24-1) → (2-(((4-(1,3-Dihydro-1-oxo-2H-isoindol-2-yl)butyl)(2-methyl-1-(1-oxopropoxy)-propoxy)phosphinyl)methyl)-4-phenylbutanoyl)-L-leucine N-phenylamide

Guidance literature:

upstream raw materials:

hexan-1-amine

1-Iodohexane

tri-n-hexylamine

Downstream raw materials:

Tetrahexylammonium picrate

tetrahexylammonium hexafluorophosphate

tetrahexylammonium hydroxide

Refernces