Technology Process of 17-(Dimethylamino)androst-4-en-3-one
There total 4 articles about 17-(Dimethylamino)androst-4-en-3-one which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
cyclohexanone; aluminum isopropoxide;
In
toluene;
a. Distillation for 30 min, b. reflux, 3h;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 66.5 percent / NaBH4 / methanol; H2O
2: 53 percent / aluminium isopropoxide, cyclohexanone / toluene / a. Distillation for 30 min, b. reflux, 3h
With
sodium tetrahydroborate; cyclohexanone; aluminum isopropoxide;
In
methanol; water; toluene;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 84.3 percent / Na, pentanol / Heating
2: 66.5 percent / NaBH4 / methanol; H2O
3: 53 percent / aluminium isopropoxide, cyclohexanone / toluene / a. Distillation for 30 min, b. reflux, 3h
With
sodium tetrahydroborate; pentan-1-ol; sodium; cyclohexanone; aluminum isopropoxide;
In
methanol; water; toluene;