Technology Process of 6-Hydroxymethyl-17β-dimethylamino-3β-pyrrolidino-5-androstene dimethiodide
There total 8 articles about 6-Hydroxymethyl-17β-dimethylamino-3β-pyrrolidino-5-androstene dimethiodide which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
In
ethanol;
Heating;
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 66.5 percent / NaBH4 / methanol; H2O
2: 53 percent / aluminium isopropoxide, cyclohexanone / toluene / a. Distillation for 30 min, b. reflux, 3h
3: 85 percent / methanol
4: 27 percent / benzene; ethanol; H2O / Ambient temperature
5: 81 percent / benzene / 4 h / Heating
6: 33 percent / NaBH4 / methanol / 2 h
7: 56 percent / ethanol / Heating
With
sodium tetrahydroborate; cyclohexanone; aluminum isopropoxide;
In
methanol; ethanol; water; toluene; benzene;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 53 percent / aluminium isopropoxide, cyclohexanone / toluene / a. Distillation for 30 min, b. reflux, 3h
2: 85 percent / methanol
3: 27 percent / benzene; ethanol; H2O / Ambient temperature
4: 81 percent / benzene / 4 h / Heating
5: 33 percent / NaBH4 / methanol / 2 h
6: 56 percent / ethanol / Heating
With
sodium tetrahydroborate; cyclohexanone; aluminum isopropoxide;
In
methanol; ethanol; water; toluene; benzene;
