N,N-dibenzyl-2-(1H-indol-3-yl)ethanaminium chloride

Base Information

Chemical Name:N,N-dibenzyl-2-(1H-indol-3-yl)ethanaminium chloride
CAS No.:63938-56-7
Molecular Formula:C24H24 N2 . Cl H
Molecular Weight:376.9217
Hs Code.:

Synonyms:1H-Indole-3-ethanamine,N,N-bis(phenylmethyl)-, monohydrochloride (9CI); Indole, 3-[2-(dibenzylamino)ethyl]-,hydrochloride (6CI,7CI)

Suppliers and Price of N,N-dibenzyl-2-(1H-indol-3-yl)ethanaminium chloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of N,N-dibenzyl-2-(1H-indol-3-yl)ethanaminium chloride

Chemical Property:

Vapor Pressure:1.21E-10mmHg at 25°C
Boiling Point:513.2°C at 760 mmHg
Flash Point:264.2°C

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of N,N-dibenzyl-2-(1H-indol-3-yl)ethanaminium chloride

There total 1 articles about N,N-dibenzyl-2-(1H-indol-3-yl)ethanaminium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 61-54-1
tryptamine

: 100-44-7
benzyl chloride

: 63938-56-7
N_b,N_b-dibenzyltryptamine hydrochloride

Guidance literature:: With potassium carbonate; potassium iodide; In N,N-dimethyl-formamide; for 24h; Ambient temperature;
DOI:10.1021/jo00058a025

Reference yield: 88.0%

: 63938-56-7
N_b,N_b-dibenzyltryptamine hydrochloride

: 98-09-9
benzenesulfonyl chloride

: 146681-87-0
N_b,N_b-N_a-(phenylsulfonyl)dibenzyltryptamine

Guidance literature:: With sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride; In toluene; for 4h; Ambient temperature;
DOI:10.1021/jo00058a025

Reference yield:

: 63938-56-7
N_b,N_b-dibenzyltryptamine hydrochloride

: 146681-86-9
2-[3-(2-Benzylamino-ethyl)-1H-indol-2-yl]-2-hydroxy-propionic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 88 percent / 40percent aq. NaOH, benzyltriethylammonium chloride / toluene / 4 h / Ambient temperature

2: 1) t-BuLi / 1) THF, pentane, below 5 deg C, 30 min, 2) below -78 deg C, 30 min

3: 88 percent / H₂ / 10percent Pd/C / acetic acid / 1.5 h

With sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride; hydrogen; tert.-butyl lithium; palladium on activated charcoal; In acetic acid; toluene;
DOI:10.1021/jo00058a025