5-(2-Bromopropyl)-1,3-benzodioxole

Base Information

Chemical Name:5-(2-Bromopropyl)-1,3-benzodioxole
CAS No.:5463-71-8
Molecular Formula:C10H11BrO2
Molecular Weight:243.1
Hs Code.:2932999099
NSC Number:15658
Mol file:5463-71-8.mol

Synonyms:5-(2-bromopropyl)-1,3-benzodioxole;5463-71-8;5-(2-Bromopropyl)benzo[d][1,3]dioxole;NSC15658;1,3-Benzodioxole, 5-(2-bromopropyl)-;AI3-20997;5-(2-bromopropyl)-1,3-dioxaindane;NSC 15658;NSC-15658;5-(2-BROMOPROPYL)-2H-1,3-BENZODIOXOLE;EN300-1997111

Suppliers and Price of 5-(2-Bromopropyl)-1,3-benzodioxole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
BROMOSAFFROLE 95.00%
5MG
$ 495.02

Total 35 raw suppliers

Chemical Property of 5-(2-Bromopropyl)-1,3-benzodioxole

Chemical Property:

Vapor Pressure:0.00452mmHg at 25°C
Boiling Point:286.5°C at 760 mmHg
Flash Point:124.3°C
PSA：18.46000
Density:1.486g/cm³
LogP:2.74120
XLogP3:3.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:241.99424
Heavy Atom Count:13
Complexity:174

Purity/Quality:

99%, ^*data from raw suppliers

BROMOSAFFROLE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(CC1=CC2=C(C=C1)OCO2)Br

Technology Process of 5-(2-Bromopropyl)-1,3-benzodioxole

There total 4 articles about 5-(2-Bromopropyl)-1,3-benzodioxole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: diethyl 4-(1-(benzo[d][1,3]dioxol-5-yl)propan-2-yl)-2,6-dimethyl-1,4-dihydropyridine-3,5-dicarboxylate

: 5463-71-8
3-<3,4-(methylenedioxy)-phenyl>-2-bromopropane

Guidance literature:: With dipotassium peroxodisulfate; tris(2,2′-bipyridyl)dichlororuthenium(II) hexahydrate; sodium bromide; In water; acetonitrile; at 20 ℃; for 24h; regioselective reaction; Sealed tube; Inert atmosphere; Irradiation;
DOI:10.1021/acs.orglett.9b01337

Reference yield:

: 94-59-7
1-allyl-3,4-methylenedioxybenzene

: 5463-71-8
3-<3,4-(methylenedioxy)-phenyl>-2-bromopropane

Guidance literature:: With water; hydrogen bromide;
DOI:10.1021/ja01301a067 DOI:10.1021/ja01198a513

Reference yield:

: 94-59-7
1-allyl-3,4-methylenedioxybenzene

: 5463-71-8
3-<3,4-(methylenedioxy)-phenyl>-2-bromopropane

: 28437-31-2
3-<3,4-(methylenedioxy)phenyl>-1-bromopropane

Guidance literature:: With borane; bromine; Yield given. Multistep reaction. Yields of byproduct given; 1.) 0 deg C, 1 h, THF, 2.) 0 deg C, 30 min, THF, H₂O;
DOI:10.1021/jo00328a025