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5463-71-8

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Basic Information
CAS No.: 5463-71-8
Name: Bromosaffrole
Article Data: 7
Molecular Structure:
Molecular Structure of 5463-71-8 (Bromosaffrole)
Formula: C10H11BrO2
Molecular Weight: 243.1
Synonyms: 5-(2-Bromopropyl)benzo[d][1,3]dioxole;3-<3,4-(methylenedioxy)-phenyl>-2-bromopropane;2-Brom-1-<3,4-methylendioxy-phenyl>-propan;5-(2-bromo-propyl)-benzo[1,3]dioxole;1,3-Benzodioxole,5-(2-bromopropyl);5-(2-Brom-propyl)-benzo[1,3]dioxol;
Density: 1.486g/cm3
Boiling Point: 286.5°C at 760 mmHg
Flash Point: 124.3°C
PSA: 18.46000
LogP: 2.74120
Related products
Synthetic route

diethyl 4-(1-(benzo[d][1,3]dioxol-5-yl)propan-2-yl)-2,6-dimethyl-1,4-dihydropyridine-3,5-dicarboxylate

5463-71-8

3-<3,4-(methylenedioxy)-phenyl>-2-bromopropane

Conditions
ConditionsYield
With dipotassium peroxodisulfate; tris(2,2′-bipyridyl)dichlororuthenium(II) hexahydrate; sodium bromide In water; acetonitrile at 20℃; for 24h; Sealed tube; Inert atmosphere; Irradiation; regioselective reaction;94%
94-59-7

1-allyl-3,4-methylenedioxybenzene

5463-71-8

3-<3,4-(methylenedioxy)-phenyl>-2-bromopropane

Conditions
ConditionsYield
With water; hydrogen bromide
94-59-7

1-allyl-3,4-methylenedioxybenzene

A

5463-71-8

3-<3,4-(methylenedioxy)-phenyl>-2-bromopropane

B

28437-31-2

3-<3,4-(methylenedioxy)phenyl>-1-bromopropane

Conditions
ConditionsYield
With borane; bromine 1.) 0 deg C, 1 h, THF, 2.) 0 deg C, 30 min, THF, H2O; Yield given. Multistep reaction. Yields of byproduct given;
5463-71-8

3-<3,4-(methylenedioxy)-phenyl>-2-bromopropane

4676-39-5

1-(1,3-benzodioxol-5-yl)-2-propanone

Conditions
ConditionsYield
With potassium hydroxide; 2-nitropropane
5463-71-8

3-<3,4-(methylenedioxy)-phenyl>-2-bromopropane

16603-18-2

(3,4,5-trimethoxyphenyl)acetone

erythro-2,3-dimethyl-4-(3,4-methylenedioxyphenyl)-1-(3,4,5-trimethoxyphenyl)-2-butanol

threo-2,3-dimethyl-4-(3,4-methylenedioxyphenyl)-1-(3,4,5-trimethoxyphenyl)-2-butanol

Conditions
ConditionsYield
With N,N,N,N,N,N-hexamethylphosphoric triamide; samarium diiodide 1.) THF, HMPA, 5 min, 2.) THF, HMPA, 25 deg C, 40 min;
With N,N,N,N,N,N-hexamethylphosphoric triamide; samarium diiodide 1.) THF, HMPA, 5 min, 2.) THF, HMPA, 25 deg C, 40 min; Yield given. Yields of byproduct given;
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