Butanoic acid, 3-(2-(4-nitrophenyl)hydrazinylidene)-, ethyl ester

Base Information

• Chemical Name: Butanoic acid, 3-(2-(4-nitrophenyl)hydrazinylidene)-, ethyl ester
• CAS No.: 63467-28-7
• Molecular Formula: C12H15N3O4
• Molecular Weight: 265.27
• European Community (EC) Number: 651-685-3
• DSSTox Substance ID: DTXSID1069877

Synonyms:63467-28-7;3-[2-(4-Nitrophenyl)hydrazono]butyric acid ethyl ester;Butanoic acid, 3-(2-(4-nitrophenyl)hydrazinylidene)-, ethyl ester;DTXSID1069877;CCG-46112;AKOS024330752;SR-01000635830-1;3-((4-NITRO-PHENYL)-HYDRAZONO)-BUTYRIC ACID ETHYL ESTER

Chemical Property of Butanoic acid, 3-(2-(4-nitrophenyl)hydrazinylidene)-, ethyl ester

Chemical Property:

• Vapor Pressure: 1.38E-06mmHg at 25°C
• Melting Point: 118 °C
• Boiling Point: 399.3°C at 760 mmHg
• PKA: 14.45±0.10(Predicted)
• Flash Point: 195.3°C
• PSA: 96.51000
• Density: 1.23g/cm³
• LogP: 2.93200
• XLogP3: 2.3
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 6
• Rotatable Bond Count: 6
• Exact Mass: 265.10625597
• Heavy Atom Count: 19
• Complexity: 343

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCOC(=O)CC(=NNC1=CC=C(C=C1)[N+](=O)[O-])C
• Isomeric SMILES: CCOC(=O)C/C(=N/NC1=CC=C(C=C1)[N+](=O)[O-])/C

Technology Process of Butanoic acid, 3-(2-(4-nitrophenyl)hydrazinylidene)-, ethyl ester

There total 3 articles about Butanoic acid, 3-(2-(4-nitrophenyl)hydrazinylidene)-, ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

ethyl acetoacetate (141-97-9) + 4-nitrophenylhydrazone (100-16-3) → 4-nitrophenylhydrazone of acetoacetic ethylester (63467-28-7)

Guidance literature:

With acetic acid; In methanol;

DOI:10.3987/COM-08-11433

Reference yield:

4,4-Dibrom-3-methyl-1-(4-nitro-phenyl)-pyrazolin-5-on (94786-81-9) → 4-nitrophenylhydrazone of acetoacetic ethylester (63467-28-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 95 percent / ethanol / Ambient temperature

2: NaI / acetic acid / 1 h

With sodium iodide; In ethanol; acetic acid;

Reference yield:

→ 4-nitrophenylhydrazone of acetoacetic ethylester (63467-28-7)

Guidance literature:

aus Acetessigsaeure-ethylester mit Hilfe von <4-Nitro-phenyl>-hydrazin;

upstream raw materials:

ethyl acetoacetate

4-nitrophenylhydrazone

4,4-Dibrom-3-methyl-1-(4-nitro-phenyl)-pyrazolin-5-on

Downstream raw materials:

5-methyl-2-(4-nitro-phenyl)-1,2-dihydro-pyrazol-3-one

ethyl 3,5-dimethyl-1-(4-nitrophenyl)-1,4,4a,5,10,10a-hexahydropyridazino<3,4-b>quinoxaline-4-carboxylate

C₁₄H₁₇N₃O₆

5-amino-3-methyl-1-(4-nitro-phenyl)-1H-pyrazole-4-carboxylic acid ethyl ester

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 63467-28-7 3-[2-(4-Nitrophenyl)hydrazono]butyric acid ethyl ester

Send

Send

Metric Ton KG G Pound L ML

Send

Send