4-(Bromomethyl)azobenzene

Base Information

Chemical Name:4-(Bromomethyl)azobenzene
CAS No.:57340-21-3
Molecular Formula:C13H11 Br N2
Molecular Weight:275.148
Hs Code.:
European Community (EC) Number:260-684-3
DSSTox Substance ID:DTXSID101269844
Nikkaji Number:J349.138B
Mol file:57340-21-3.mol

Synonyms:4-(Bromomethyl)azobenzene;57340-21-3;[4-(bromomethyl)phenyl]-phenyldiazene;EINECS 260-684-3;MFCD18974165;(e)-1-[4-(bromomethyl)phenyl]-2-phenyldiazene;4-(bromomethyl) azobenzene;DTXSID101269844;AC6386;AKOS040824674;SY237645;1-[4-(Bromomethyl)phenyl]-2-phenyldiazene;10.14272/DFGWIAOSYURBRH-FOCLMDBBSA-N.1;A923150;doi:10.14272/DFGWIAOSYURBRH-FOCLMDBBSA-N.1

Suppliers and Price of 4-(Bromomethyl)azobenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

AK Scientific
4-(Bromomethyl)azobenzene
250mg
$ 262.00

Total 8 raw suppliers

Chemical Property of 4-(Bromomethyl)azobenzene

Chemical Property:

Vapor Pressure:1.36E-05mmHg at 25°C
Boiling Point:378.5°Cat760mmHg
Flash Point:182.7°C
PSA：24.72000
Density:1.33g/cm³
LogP:4.99690
XLogP3:4.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:274.01056
Heavy Atom Count:16
Complexity:216

Purity/Quality:

97% ^*data from raw suppliers

4-(Bromomethyl)azobenzene ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)N=NC2=CC=C(C=C2)CBr

Technology Process of 4-(Bromomethyl)azobenzene

There total 12 articles about 4-(Bromomethyl)azobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.6%

: 949-87-1
4-Methylazobenzol

: 57340-21-3
1-(4-(bromomethyl)phenyl)-2-phenyldiazene

Guidance literature:: With N-Bromosuccinimide; dibenzoyl peroxide; In tetrachloromethane; for 4h; Inert atmosphere; Reflux;

Reference yield: 91.0%

: 65926-74-1
1-(4-(hydroxymethyl)phenyl)-2-phenyldiazene

: 57340-21-3
1-(4-(bromomethyl)phenyl)-2-phenyldiazene

Guidance literature:: With N-Bromosuccinimide; triphenylphosphine; In tetrahydrofuran; at 20 ℃; for 12h;
DOI:10.1002/chem.201102609

Reference yield:

: 586-96-9
Nitrosobenzene

: 57340-21-3
1-(4-(bromomethyl)phenyl)-2-phenyldiazene

Guidance literature:: Multi-step reaction with 2 steps

1: ethanol; acetic acid

2: phosphorus (III)-bromide; benzene

With ethanol; phosphorus tribromide; acetic acid; benzene;