3-Oxo-N-(4-pyridylsulphonyl)butyramide N-oxide

Base Information

• Chemical Name: 3-Oxo-N-(4-pyridylsulphonyl)butyramide N-oxide
• CAS No.: 85153-50-0
• Molecular Formula: C9H10N2O5S
• Molecular Weight: 258.255
• Mol file: 85153-50-0.mol

Synonyms:acetoacetyl-(1-oxy-pyridine-4-sulfonyl)-amine;N-Acetoacetyl-4-pyridinsulfonamid-1-oxid;3-oxo-N-(4-pyridylsulfonyl)butyramide N-oxide;1-Oxy-pyridine-4-sulfonic acid (3-oxo-butyryl)-amide;Acetoacetyl-(1-oxy-pyridin-4-sulfonyl)-amin;

Chemical Property of 3-Oxo-N-(4-pyridylsulphonyl)butyramide N-oxide

Chemical Property:

• PSA: 114.15000
• Density: 1.46g/cm³
• LogP: 1.37080

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-Oxo-N-(4-pyridylsulphonyl)butyramide N-oxide

There total 3 articles about 3-Oxo-N-(4-pyridylsulphonyl)butyramide N-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-pyridinethione (19829-29-9) → 3-oxo-N-(1-oxy-pyridine-4-sulfonyl)-butyramide (85153-50-0)

Guidance literature:

Multi-step reaction with 2 steps

1: chlorine; aqueous HCl; ice; aqueous NH₃ / -5 - 0 °C / Reaktion ueber mehrere Stufen

2: aqueous NaOH; acetone / <10

With hydrogenchloride; ammonium hydroxide; sodium hydroxide; Methamphetamin; chlorine; acetone;

Reference yield:

4-methyleneoxetan-2-one (674-82-8,2130-41-8) + pyridine-4-sulfonamide N-oxide (75903-65-0) → 3-oxo-N-(1-oxy-pyridine-4-sulfonyl)-butyramide (85153-50-0)

Guidance literature:

With sodium hydroxide; acetone;

Reference yield:

→ 3-oxo-N-(1-oxy-pyridine-4-sulfonyl)-butyramide (85153-50-0)

Guidance literature:

4-Pyridin-sulfonamid-1-oxid, dimeres Keten;

upstream raw materials:

4-methyleneoxetan-2-one

pyridine-4-sulfonamide N-oxide

4-pyridinethione

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