Morpholine, 4-(2-(2,4-dichlorophenyl)-1-oxo-2-propenyl)-

Base Information

Chemical Name:Morpholine, 4-(2-(2,4-dichlorophenyl)-1-oxo-2-propenyl)-
CAS No.:108664-51-3
Molecular Formula:C₁₃H₁₃Cl₂NO₂
Molecular Weight:286.158
Hs Code.:
DSSTox Substance ID:DTXSID00148698
Wikidata:Q83014295
ChEMBL ID:CHEMBL35452
Mol file:108664-51-3.mol

Synonyms:108664-51-3;Morpholine, 4-(2-(2,4-dichlorophenyl)-1-oxo-2-propenyl)-;Morpholine, 4-[2-(2,4-dichlorophenyl)-1-oxo-2-propenyl]-;CHEMBL35452;DTXSID00148698;2-(2,4-dichlorophenyl)-1-morpholino-prop-2-en-1-one

Suppliers and Price of Morpholine, 4-(2-(2,4-dichlorophenyl)-1-oxo-2-propenyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Morpholine, 4-(2-(2,4-dichlorophenyl)-1-oxo-2-propenyl)-

Chemical Property:

Vapor Pressure:9.58E-10mmHg at 25°C
Boiling Point:489.9°C at 760 mmHg
Flash Point:250.1°C
Density:1.316g/cm³
XLogP3:2.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:285.0323340
Heavy Atom Count:18
Complexity:329

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C=C(C1=C(C=C(C=C1)Cl)Cl)C(=O)N2CCOCC2

Technology Process of Morpholine, 4-(2-(2,4-dichlorophenyl)-1-oxo-2-propenyl)-

There total 4 articles about Morpholine, 4-(2-(2,4-dichlorophenyl)-1-oxo-2-propenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6306-60-1
2,4-Dichlorophenylacetonitrile

: 108664-51-3
2-(2,4-Dichloro-phenyl)-1-morpholin-4-yl-propenone

Guidance literature:: Multi-step reaction with 4 steps

1: 64 percent / Ac₂O / 2.5 h / 70 °C

2: 85 percent / 98percent H₂SO₄ / H₂O / 15 h / 130 °C

3: SOCl₂ / 0.5 h / 50 °C

4: ET₃N / CH₂Cl₂ / 0.25 h / Ambient temperature

With thionyl chloride; sulfuric acid; acetic anhydride; triethylamine; In dichloromethane; water;
DOI:10.1021/jm00391a037

Reference yield:

: 26923-38-6
2-(2,4-Dichloro-phenyl)-acrylonitrile

: 108664-51-3
2-(2,4-Dichloro-phenyl)-1-morpholin-4-yl-propenone

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / 98percent H₂SO₄ / H₂O / 15 h / 130 °C

2: SOCl₂ / 0.5 h / 50 °C

3: ET₃N / CH₂Cl₂ / 0.25 h / Ambient temperature

With thionyl chloride; sulfuric acid; triethylamine; In dichloromethane; water;
DOI:10.1021/jm00391a037

Reference yield:

: 108664-84-2
2-(2,4-dichlorophenyl)acrylate

: 108664-51-3
2-(2,4-Dichloro-phenyl)-1-morpholin-4-yl-propenone

Guidance literature:: Multi-step reaction with 2 steps

1: SOCl₂ / 0.5 h / 50 °C

2: ET₃N / CH₂Cl₂ / 0.25 h / Ambient temperature

With thionyl chloride; triethylamine; In dichloromethane;
DOI:10.1021/jm00391a037