3,5-Dichloropyridin-4-ol

Base Information

Chemical Name:3,5-Dichloropyridin-4-ol
CAS No.:17228-70-5
Molecular Formula:C5H3Cl2NO
Molecular Weight:163.991
Hs Code.:2933399090
European Community (EC) Number:241-268-0,241-267-5
DSSTox Substance ID:DTXSID60938118
Nikkaji Number:J256.529C,J318.183I
Wikidata:Q72466444
Mol file:17228-70-5.mol

Synonyms:3,5-Dichloropyridin-4-ol;3,5-Dichloro-4-hydroxypyridine;17228-70-5;17228-71-6;3,5-dichloro-1H-pyridin-4-one;3,5-dichloropyridin-4(1H)-one;3,5-Dichloro-4-pyridone;3,5-Dichloro-4-pyridinol;4(1H)-Pyridinone, 3,5-dichloro-;EINECS 241-267-5;EINECS 241-268-0;3,5-dichloro-1,4-dihydropyridin-4-one;3,5-DICHLORO-4-PYRIDINOL 3,5-DICHLORO-4-HYDROXYPYRIDINE SPECIALITY CHEMICALS;MFCD00051673;4-PYRIDINOL, 3,5-DICHLORO-;OXAZOLE,2-METHYL-;3,5-Dichloro-pyridin-4-ol;F2124-0020;SCHEMBL2681685;DTXSID60938118;4(1H)-Pyridone, 3,5-dichloro-;3,5-Dichloro-4(1H)-pyridinone #;MFCD00047448;AKOS002666023;AKOS005208203;Pyridin-4(1H)-one, 3,5-dichloro-;AB02053;AC-4669;DS-1252;PS-5913;SB52551;A3796;CS-0018965;FT-0614545;FT-0614546;EN300-235699;A881885;W-107866;F1957-0005

Suppliers and Price of 3,5-Dichloropyridin-4-ol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
3,5-Dichloropyridin-4(1H)-one
10g
$ 70.00

TCI Chemical
3,5-Dichloro-4-hydroxypyridine >98.0%(T)
25g
$ 67.00

SynQuest Laboratories
3,5-Dichloropyridin-4(1H)-one
1 g
$ 16.00

SynQuest Laboratories
3,5-Dichloropyridin-4(1H)-one
5 g
$ 29.00

Matrix Scientific
3,5-Dichloro-4-hydroxypyridine 98%
25g
$ 58.00

Matrix Scientific
3,5-Dichloro-4-hydroxypyridine 98%
100g
$ 176.00

Crysdot
3,5-Dichloropyridin-4(1H)-one 98%
500g
$ 470.00

Chemenu
3,5-Dichloro-4-hydroxypyridine 98%
500g
$ 439.00

Biosynth Carbosynth
3,5-Dichloro-4-hydroxypyridine
100 g
$ 178.00

Biosynth Carbosynth
3,5-Dichloro-4-hydroxypyridine
50 g
$ 111.00

Total 70 raw suppliers

Chemical Property of 3,5-Dichloropyridin-4-ol

Chemical Property:

Appearance/Colour:white to off-white solid
Vapor Pressure:0.0616mmHg at 25°C
Melting Point:56-59 °C(lit.)
Refractive Index:1.605
Boiling Point:242.6 °C at 760 mmHg
PKA:7.31±0.69(Predicted)
Flash Point:100.5 °C
PSA：33.12000
Density:1.52 g/cm³
LogP:2.09400
Storage Temp.:Sealed in dry,Room Temperature
Solubility.:DMSO (Slightly)
XLogP3:1.8
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:0
Exact Mass:162.9591691
Heavy Atom Count:9
Complexity:187

Purity/Quality:

99%, ^*data from raw suppliers

3,5-Dichloropyridin-4(1H)-one ^*data from reagent suppliers

Safty Information:

Pictogram(s): Xn
Hazard Codes:Xn,Xi
Statements: 22-36/37/38
Safety Statements: 36/37/39-26-22-36

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=C(C(=O)C(=CN1)Cl)Cl

Technology Process of 3,5-Dichloropyridin-4-ol

There total 1 articles about 3,5-Dichloropyridin-4-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 108-96-3,26266-70-6
4-pyridone

: 17228-70-5
3,5-dichloropyridin-4-one

Guidance literature:: With sodium hypochlorite; In chloroform; for 0.00833333h;
DOI:10.1021/jo00199a008

Reference yield: 98.0%

: 17228-70-5
3,5-dichloropyridin-4-one

: 7154-66-7
2-bromobenzoic acid chloride

: 1-(2-bromo-benzoyl)-3,5-dichloro-1H-pyridin-4-one

Guidance literature:: With sodium hydride; In tetrahydrofuran; at 20 ℃;
DOI:10.1016/S0040-4039(99)01542-7

Reference yield: 93.0%

: 17228-70-5
3,5-dichloropyridin-4-one

: 72038-68-7
(hexa-4,5-dien-1-yl)benzene

: C₁₇H₁₇Cl₂NO

Guidance literature:: With chloro(1,5-cyclooctadiene)rhodium(I) dimer; C₃₆H₅₈FeP₂; In 1,2-dichloro-ethane; at 80 ℃; for 18h; stereoselective reaction; Inert atmosphere; Schlenk technique; Sealed tube;
DOI:10.1002/chem.201701382