2-METHYL-PARA-AMINOBENZOICACID

Base Information

• Chemical Name: 2-METHYL-PARA-AMINOBENZOICACID
• CAS No.: 38667-55-9
• Molecular Formula: C9H8ClNO3
• Molecular Weight: 213.62
• Hs Code.: 2924299090
• Mol file: 38667-55-9.mol

Synonyms:2-Chlor-4-acetamino-benzoesaeure;4-acetamido-2-chloro-benzoic Acid;4-Acetylamino-2-chlor-benzoesaeure;4-Acetamino-2-chlorobenzoesaeure;2-Chlor-4-acetylaminobenzoesaeure;2-chloro-4-acetamidobenzoic acid;

Chemical Property of 2-METHYL-PARA-AMINOBENZOICACID

Chemical Property:

• Vapor Pressure: 1.07E-08mmHg at 25°C
• Boiling Point: 444.9°C at 760 mmHg
• Flash Point: 222.9°C
• PSA: 66.40000
• Density: 1.453g/cm³
• LogP: 2.06960

Purity/Quality:

98% ^*data from raw suppliers

4-(acetylamino)-2-chlorobenzoicAcid ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-METHYL-PARA-AMINOBENZOICACID

There total 9 articles about 2-METHYL-PARA-AMINOBENZOICACID which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.1%

N-(3-chloro-4-methylphenyl)acetamide (7149-79-3) → 4-Acetylamino-2-chlorobenzoic acid (38667-55-9)

Guidance literature:

With oxygen; cobalt(II) acetate; sodium bromide; In acetic acid; at 100 ℃; for 1.33333h;

Reference yield:

4-amino-2-chlorobenzoic acid (2457-76-3) + acetyl chloride (75-36-5) → 4-Acetylamino-2-chlorobenzoic acid (38667-55-9)

Guidance literature:

With triethylamine; In tetrahydrofuran; dichloromethane;

Reference yield:

acetic acid-(3-chloro-4-chloroacetyl-anilide) (90798-26-8) → 4-Acetylamino-2-chlorobenzoic acid (38667-55-9)

Guidance literature:

With permanganate(VII) ion; magnesium sulfate; at 85 - 90 ℃;

upstream raw materials:

N-(3-chloro-4-methylphenyl)acetamide

N-(3-chloro-4-formylphenyl)acetamide

acetic acid-(4-acetyl-3-chloro-anilide)

acetic acid-(3-chloro-4-chloroacetyl-anilide)

Downstream raw materials:

methyl 4-amino-2-chlorobenzoate

ethyl-2-chloro-4-amino-benzoate

4-amino-2-chlorobenzoic acid

N(3'-nitrophenyl)-4-acetylaminoanthranilic acid

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