Carbamic acid, N-(3-(diethylamino)propyl)dithio-

Base Information

• Chemical Name: Carbamic acid, N-(3-(diethylamino)propyl)dithio-
• CAS No.: 19022-72-1
• Molecular Formula: C8H18N2S2
• Molecular Weight: 0
• Hs Code.: 2930909090
• DSSTox Substance ID: DTXSID10172500
• Nikkaji Number: J42.882E
• Mol file: 19022-72-1.mol

Synonyms:19022-72-1;BRN 1763523;3-(diethylamino)propylcarbamodithioic acid;CARBAMIC ACID, N-(3-(DIETHYLAMINO)PROPYL)DITHIO-;N-[3-(Diethylamino)propyl]carbamodithioic acid;N-(3-(Diethylamino)propyl)dithiocarbamic acid;3-04-00-00562 (Beilstein Handbook Reference);DTXSID10172500;LS-49297;Carbamodithioic acid, [3-(diethylamino)propyl]-

Chemical Property of Carbamic acid, N-(3-(diethylamino)propyl)dithio-

Chemical Property:

• Vapor Pressure: 0.00685mmHg at 25°C
• Refractive Index: 1.542
• Boiling Point: 270.4°C at 760 mmHg
• Flash Point: 117.3°C
• PSA: 93.20000
• Density: 1.054g/cm³
• LogP: 1.93390
• XLogP3: 1.9
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 6
• Exact Mass: 206.09114093
• Heavy Atom Count: 12
• Complexity: 124

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: CCN(CC)CCCNC(=S)S

Technology Process of Carbamic acid, N-(3-(diethylamino)propyl)dithio-

There total 3 articles about Carbamic acid, N-(3-(diethylamino)propyl)dithio- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

carbon disulfide (75-15-0,12122-00-8) + diethylaminopropylamine (104-78-9) → N-(2-diethylaminopropyl)-dithiocarbamic acid (19022-72-1)

Guidance literature:

In diethyl ether;

Reference yield:

diethylaminopropylamine (104-78-9) → N-(2-diethylaminopropyl)-dithiocarbamic acid (19022-72-1)

Guidance literature:

With diethyl ether;

Reference yield:

3-diethylaminopropyl chloride (104-77-8) → N-(2-diethylaminopropyl)-dithiocarbamic acid (19022-72-1)

Guidance literature:

Multi-step reaction with 2 steps

1: xylene / Hydrolyse des entstandenen N-<3-Diaethylamino-propyl>-phthalimids mit konz.HCl bei Siedetemperatur_.

2: diethyl ether

With diethyl ether; xylene;

upstream raw materials:

carbon disulfide

diethylaminopropylamine

3-diethylaminopropyl chloride

Downstream raw materials:

3-(N,N-diethylamino)propyl isothiocyanate

Refernces

• 1、 Muftic,Hoyer. "Alkylaminoalkyl-dithiocarbamic acids, new drugs against Pityrosporum ovale.". . p. 1205 - 1207. Retrieved 2007/10/06.