Ethanaminium, 2-(acetyloxy)-N,N-dimethyl-N-((triethylsilyl)methyl)-, iodide

Base Information

• Chemical Name: Ethanaminium, 2-(acetyloxy)-N,N-dimethyl-N-((triethylsilyl)methyl)-, iodide
• CAS No.: 84584-66-7
• Molecular Formula: C₁₃H₃₀NO₂Si*I
• Molecular Weight: 387.377
• DSSTox Substance ID: DTXSID801004865
• Mol file: 84584-66-7.mol

Synonyms:Dimethyl(2-hydroxyethyl)(triethylsilylmethyl)ammonium iodide acetate (ester);Ammonium, dimethyl(2-hydroxyethyl)(triethylsilylmethyl)-, iodide, acetate (ester);Ethanaminium, 2-(acetyloxy)-N,N-dimethyl-N-((triethylsilyl)methyl)-, iodide;84584-66-7;C13H30NO2Si.I;C13-H30-N-O2-Si.I;DTXSID801004865;LS-17787;2-(Acetyloxy)-N,N-dimethyl-N-[(triethylsilyl)methyl]ethan-1-aminium iodide

Chemical Property of Ethanaminium, 2-(acetyloxy)-N,N-dimethyl-N-((triethylsilyl)methyl)-, iodide

Chemical Property:

• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 9
• Exact Mass: 387.10905
• Heavy Atom Count: 18
• Complexity: 229

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC[Si](CC)(CC)C[N+](C)(C)CCOC(=O)C.[I-]

Technology Process of Ethanaminium, 2-(acetyloxy)-N,N-dimethyl-N-((triethylsilyl)methyl)-, iodide

There total 2 articles about Ethanaminium, 2-(acetyloxy)-N,N-dimethyl-N-((triethylsilyl)methyl)-, iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

Acetic acid 2-(methyl-triethylsilanylmethyl-amino)-ethyl ester (84584-59-8) + methyl iodide (74-88-4) → (2-Acetoxy-ethyl)-dimethyl-triethylsilanylmethyl-ammonium; iodide (84584-66-7)

Guidance literature:

In diethyl ether; 1.) 35-40 deg C, 4 h, 2.) ca. 20 deg C, 16 h;

DOI:10.1007/BF00772158

Reference yield:

Triethyl<(N-methyl-N-2-hydroxyethyl)aminomethyl>silane (21654-71-7) → (2-Acetoxy-ethyl)-dimethyl-triethylsilanylmethyl-ammonium; iodide (84584-66-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 52 percent / Et₃N / diethyl ether / 3 h / Heating

2: 80 percent / diethyl ether / 1.) 35-40 deg C, 4 h, 2.) ca. 20 deg C, 16 h

With triethylamine; In diethyl ether;

DOI:10.1007/BF00772158

upstream raw materials:

Acetic acid 2-(methyl-triethylsilanylmethyl-amino)-ethyl ester

methyl iodide

Triethyl<(N-methyl-N-2-hydroxyethyl)aminomethyl>silane