Pentanedioic acid, 3,3-dicyano-, 1,5-diethyl ester

Base Information

Chemical Name:Pentanedioic acid, 3,3-dicyano-, 1,5-diethyl ester
CAS No.:77415-69-1
Molecular Formula:C11H14N2O4
Molecular Weight:238.2399
Hs Code.:2926909090
Mol file:77415-69-1.mol

Synonyms:diethyl 3,3-dicyanoglutarate;

Suppliers and Price of Pentanedioic acid, 3,3-dicyano-, 1,5-diethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
Diethyl3,3-dicyanopentanedioate 95+%
1g
$ 589.00

Total 7 raw suppliers

Chemical Property of Pentanedioic acid, 3,3-dicyano-, 1,5-diethyl ester

Chemical Property:

Vapor Pressure:9.82E-07mmHg at 25°C
Boiling Point:403.9°C at 760 mmHg
Flash Point:176.7°C
PSA：100.18000
Density:1.168g/cm³
LogP:0.92636

Purity/Quality:

99% ^*data from raw suppliers

Diethyl3,3-dicyanopentanedioate 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Pentanedioic acid, 3,3-dicyano-, 1,5-diethyl ester

There total 1 articles about Pentanedioic acid, 3,3-dicyano-, 1,5-diethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.2%

: 105-36-2
ethyl bromoacetate

: 109-77-3
malononitrile

: 77415-69-1
diethyl 3,3-dicyanoglutarate

Guidance literature:: With sodium carbonate; In ethanol; at 20 ℃; for 48h;

Reference yield: 32.0%

: 77415-69-1
diethyl 3,3-dicyanoglutarate

: 82379-18-8,84296-36-6,947239-51-2
2,7-diazaspiro<4.4>nonane-3,8-dione

Guidance literature:: With hydrogen; triethylamine; cobalt; In N,N-dimethyl-formamide; for 23h; under 124116 - 279260 Torr;
DOI:10.1021/jm00170a035

Reference yield:

: 77415-69-1
diethyl 3,3-dicyanoglutarate

: 77415-72-6
2,7-bis(phenylmethyl)-2,7-diazaspiro<4.4>nonane

Guidance literature:: Multi-step reaction with 3 steps

1: 93 percent / conc. H₂SO₄ / acetic acid / 0.5 h / Heating

2: 1.) sodium hydroxide, 2.) / 1.) ethanol, room temp., 2 h, 2.) DMF, 80-90 deg C, 24 h

3: lithium aluminum hydride / tetrahydrofuran / 36 h / Heating

With sodium hydroxide; lithium aluminium tetrahydride; sulfuric acid; In tetrahydrofuran; acetic acid;
DOI:10.1021/jo00326a031