Benzo[4,5]cyclohept[1,2-b]indole

Base Information

Chemical Name:Benzo[4,5]cyclohept[1,2-b]indole
CAS No.:242-14-8
Molecular Formula:C17H11N
Molecular Weight:229.281
Hs Code.:
NSC Number:73037
DSSTox Substance ID:DTXSID00291077

Synonyms:242-14-8;Benzo[4,5]cyclohept[1,2-b]indole;Benzo[4,2-b]indole;NSC73037;SCHEMBL4514971;DTXSID00291077;NSC-73037

Suppliers and Price of Benzo[4,5]cyclohept[1,2-b]indole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of Benzo[4,5]cyclohept[1,2-b]indole

Chemical Property:

Vapor Pressure:1.7E-06mmHg at 25°C
Boiling Point:408.1°C at 760 mmHg
Flash Point:193.1°C
Density:1.16g/cm³
XLogP3:4.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:0
Exact Mass:229.089149355
Heavy Atom Count:18
Complexity:300

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C2C=C3C(=NC4=CC=CC=C43)C=CC2=C1

Technology Process of Benzo[4,5]cyclohept[1,2-b]indole

There total 8 articles about Benzo[4,5]cyclohept[1,2-b]indole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 131832-67-2
1,4,7,8-tetrahydro-1-azadibenzazulene

: 225-11-6
benz[a]acridine

: 242-14-8
benzo[4,5]cyclohePt[1,2-b]indole

Guidance literature:: at 330 ℃;
DOI:10.1021/ja01609a061

Reference yield:

: 131832-67-2
1,4,7,8-tetrahydro-1-azadibenzazulene

: 242-14-8
benzo[4,5]cyclohePt[1,2-b]indole

Guidance literature:: With palladium on activated charcoal;
DOI:10.1021/ja01609a061

Reference yield:

: 17532-66-0
ethyl 2-[2-(2-ethoxy-2-oxoethyl)phenyl]acetate

: 242-14-8
benzo[4,5]cyclohePt[1,2-b]indole

Guidance literature:: Multi-step reaction with 7 steps

1: LiAlH₄; diethyl ether

2: aqueous hydrobromic acid

4: phenyl lithium; N-methyl-aniline; diethyl ether

5: H₂SO₄

6: acetic acid

7: tetrachloro-<1,4>benzoquinone; benzene

With lithium aluminium tetrahydride; diethyl ether; sulfuric acid; hydrogen bromide; chloranil; acetic acid; phenyllithium; N-methylaniline; benzene;
DOI:10.1021/ja01609a061