1,5-Bis(p-methoxyphenyl)-3,7-diazaadamantan-9-one

Base Information

Chemical Name:1,5-Bis(p-methoxyphenyl)-3,7-diazaadamantan-9-one
CAS No.:69352-68-7
Molecular Formula:C₂₂H₂₄N₂O₃
Molecular Weight:364.444
Hs Code.:
Mol file:69352-68-7.mol

Synonyms:5,7-bis-(4-methoxy-phenyl)-1,3-diaza-adamantan-6-one;5,7-Bis-(4-methoxy-phenyl)-1,3-diaza-tricyclo[3.3.1.13,7]decan-6-one;1,5-Bis-(4-methoxy-phenyl)-3,7-diaza-adamantanon-(9);

Suppliers and Price of 1,5-Bis(p-methoxyphenyl)-3,7-diazaadamantan-9-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 3 raw suppliers

Chemical Property of 1,5-Bis(p-methoxyphenyl)-3,7-diazaadamantan-9-one

Chemical Property:

Vapor Pressure:1.13E-11mmHg at 25°C
Melting Point:219 - 220 °C
Boiling Point:538.7°C at 760 mmHg
Flash Point:279.6°C
PSA：42.01000
Density:1.3g/cm³
LogP:1.92680

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of 1,5-Bis(p-methoxyphenyl)-3,7-diazaadamantan-9-one

There total 3 articles about 1,5-Bis(p-methoxyphenyl)-3,7-diazaadamantan-9-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 29903-09-1
1,3-bis(4-methoxyphenyl)acetone

: 69352-68-7
5,7-bis(4-methoxyphenyl)-1,3-diazatricyclo<3.3.1.1^3,7>decan-6-one

Guidance literature:: With ammonium acetate; In ethanol; for 5h; Heating;
DOI:10.1002/hlca.19940770320

Reference yield:

: 104-01-8
4-Methoxyphenylacetic acid

: 69352-68-7
5,7-bis(4-methoxyphenyl)-1,3-diazatricyclo<3.3.1.1^3,7>decan-6-one

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) MnCl₂*4H₂O, Na₂CO₃ / 1.) H₂O, 2.) 200-250 deg C, 0.5 Torr

2: 72 percent / NH₄OAc / ethanol / 5 h / Heating

With ammonium acetate; sodium carbonate; manganese(ll) chloride; In ethanol;
DOI:10.1002/hlca.19940770320