1-(2,4-Dinitrophenyl)-2-(9h-fluoren-9-ylidene)hydrazine

Base Information

Chemical Name:1-(2,4-Dinitrophenyl)-2-(9h-fluoren-9-ylidene)hydrazine
CAS No.:15884-61-4
Molecular Formula:C19H12 N4 O4
Molecular Weight:360.329
Hs Code.:
NSC Number:24100
DSSTox Substance ID:DTXSID90282075
Nikkaji Number:J590.688A
Mol file:15884-61-4.mol

Synonyms:15884-61-4;1-(2,4-dinitrophenyl)-2-(9h-fluoren-9-ylidene)hydrazine;NSC24100;DTXSID90282075;NSC-24100;AKOS004902038;9h-fluoren-9-one (2,4-dinitrophenyl)hydrazone (en);N-(2,4-DINITRO-PHENYL)-N'-FLUOREN-9-YLIDENE-HYDRAZINE

Suppliers and Price of 1-(2,4-Dinitrophenyl)-2-(9h-fluoren-9-ylidene)hydrazine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 7 raw suppliers

Chemical Property of 1-(2,4-Dinitrophenyl)-2-(9h-fluoren-9-ylidene)hydrazine

Chemical Property:

Vapor Pressure:9.04E-14mmHg at 25°C
Boiling Point:587.2°C at 760 mmHg
Flash Point:308.9°C
Density:1.47g/cm³
XLogP3:5.4
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:2
Exact Mass:360.08585488
Heavy Atom Count:27
Complexity:590

Purity/Quality:: 98%min ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C2C(=C1)C3=CC=CC=C3C2=NNC4=C(C=C(C=C4)[N+](=O)[O-])[N+](=O)[O-]

Technology Process of 1-(2,4-Dinitrophenyl)-2-(9h-fluoren-9-ylidene)hydrazine

There total 7 articles about 1-(2,4-Dinitrophenyl)-2-(9h-fluoren-9-ylidene)hydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 486-25-9,952573-42-1
9-fluorenone

: 119-26-6
(2,4-dinitro-phenyl)-hydrazine

: 15884-61-4
fluorenone-2,4-dinitrophenylhydrazone

Guidance literature:

Reference yield:

: 1689-64-1
9-Fluorenol

: 15884-61-4
fluorenone-2,4-dinitrophenylhydrazone

Guidance literature:: Multi-step reaction with 2 steps

1: 1-chlorobenzotriazole / acetic acid; H2O / 30 °C / substituted fluoren-9-ols, other temperatures, ΔH(excit.), ΔS(excit.), E(activ.)

2: 70 percent

With N-chlorobenzotriazole; In water; acetic acid;

Reference yield:

: 832-80-4
9-diazofluorenone

: 15884-61-4
fluorenone-2,4-dinitrophenylhydrazone

Guidance literature:: Multi-step reaction with 2 steps

1: 135 - 140 °C

2: (i) O₃, (ii) Me₂S, MeOH, (iii) /BRN= 615586/

DOI:10.1021/ja00827a031