N,N'-Bis(4-(2-methylpiperidino)but-2-ynyl)-1,2,4,5-benzenetetracarboxylic 1,2:4,5-diimide

Base Information

Chemical Name:N,N'-Bis(4-(2-methylpiperidino)but-2-ynyl)-1,2,4,5-benzenetetracarboxylic 1,2:4,5-diimide
CAS No.:77763-00-9
Molecular Formula:C₃₀H₃₄N₄O₄
Molecular Weight:514.624
Hs Code.:
DSSTox Substance ID:DTXSID40998957
Nikkaji Number:J62.212E

Synonyms:BRN 5677372;1,2,4,5-Benzenetetracarboxylic 1,2:4,5-diimide, N,N'-bis(4-(2-methylpiperidino)but-2-ynyl)-;N,N'-Bis(4-(2-methylpiperidino)but-2-ynyl)-1,2,4,5-benzenetetracarboxylic 1,2:4,5-diimide;77763-00-9;DTXSID40998957;LS-32171;N,N'-Bis[4-(2-methylpiperidino)-2-butynyl]benzene-1,2:4,5-bis(dicarbimide);2,6-Bis[4-(2-methylpiperidin-1-yl)but-2-yn-1-yl]pyrrolo[3,4-f]isoindole-1,3,5,7(2H,6H)-tetrone

Suppliers and Price of N,N'-Bis(4-(2-methylpiperidino)but-2-ynyl)-1,2,4,5-benzenetetracarboxylic 1,2:4,5-diimide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,N'-Bis(4-(2-methylpiperidino)but-2-ynyl)-1,2,4,5-benzenetetracarboxylic 1,2:4,5-diimide

Chemical Property:

Vapor Pressure:1.97E-18mmHg at 25°C
Boiling Point:681.6°C at 760 mmHg
Flash Point:286.7°C
Density:1.253g/cm³
XLogP3:2.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:4
Exact Mass:514.25800558
Heavy Atom Count:38
Complexity:994

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1CCCCN1CC#CCN2C(=O)C3=CC4=C(C=C3C2=O)C(=O)N(C4=O)CC#CCN5CCCCC5C

Technology Process of N,N'-Bis(4-(2-methylpiperidino)but-2-ynyl)-1,2,4,5-benzenetetracarboxylic 1,2:4,5-diimide

There total 2 articles about N,N'-Bis(4-(2-methylpiperidino)but-2-ynyl)-1,2,4,5-benzenetetracarboxylic 1,2:4,5-diimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 18158-82-2
2,6-di-prop-2-ynyl-pyrrolo[3,4-f]isoindole-1,3,5,7-tetraone

: 109-05-7,3000-79-1
2-Methylpiperidin

: 77763-00-9
2,6-Bis-[4-(2-methyl-piperidin-1-yl)-but-2-ynyl]-pyrrolo[3,4-f]isoindole-1,3,5,7-tetraone

Guidance literature:: With copper(l) chloride; In 1,4-dioxane; for 3h; Heating;

Reference yield:

: 2550-73-4
pyrrolo[3,4-f]isoindole-1,3,5,7-tetraone

: 77763-00-9
2,6-Bis-[4-(2-methyl-piperidin-1-yl)-but-2-ynyl]-pyrrolo[3,4-f]isoindole-1,3,5,7-tetraone

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) potassium hydroxide, 65 percent alcohol / 1.) DMF, 1 h, r.t.; 2.) DMF, 70-80 deg C, 16 h

2: 51 percent / cuprous chloride / dioxane / 3 h / Heating

With potassium hydroxide; ethanol; copper(l) chloride; In 1,4-dioxane;