1-[3-(5-Acetyl-2,3-dimethoxyphenyl)-4,5-dimethoxyphenyl]ethanone

Base Information

Chemical Name:1-[3-(5-Acetyl-2,3-dimethoxyphenyl)-4,5-dimethoxyphenyl]ethanone
CAS No.:55919-72-7
Molecular Formula:C20H22 O6
Molecular Weight:358.391
Hs Code.:
NSC Number:43328
DSSTox Substance ID:DTXSID30285964
Nikkaji Number:J987.543C
Wikidata:Q82021523
Mol file:55919-72-7.mol

Synonyms:55919-72-7;1-[3-(5-acetyl-2,3-dimethoxyphenyl)-4,5-dimethoxyphenyl]ethanone;NSC43328;FLAVANONE,7-DIHYDROXY-;DTXSID30285964;NSC-43328;5,5'-diacetyl-2,2',3,3'-tetramethoxy-1,1'-biphenyl;1,1'-(5,5',6,6'-Tetramethoxy[1,1'-biphenyl]-3,3'-diyl)di(ethan-1-one);1-[3-(5-ACETYL-2,3-DIMETHOXY-PHENYL)-4,5-DIMETHOXY-PHENYL]ETHANONE

Suppliers and Price of 1-[3-(5-Acetyl-2,3-dimethoxyphenyl)-4,5-dimethoxyphenyl]ethanone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 1-[3-(5-Acetyl-2,3-dimethoxyphenyl)-4,5-dimethoxyphenyl]ethanone

Chemical Property:

Melting Point:138-139 °C
Boiling Point:482.6±45.0 °C(Predicted)
Flash Point:210.4oC
PSA：71.06000
Density:1.142±0.06 g/cm3(Predicted)
LogP:3.79320
XLogP3:2.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:7
Exact Mass:358.14163842
Heavy Atom Count:26
Complexity:449

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=O)C1=CC(=C(C(=C1)OC)OC)C2=C(C(=CC(=C2)C(=O)C)OC)OC

Technology Process of 1-[3-(5-Acetyl-2,3-dimethoxyphenyl)-4,5-dimethoxyphenyl]ethanone

There total 1 articles about 1-[3-(5-Acetyl-2,3-dimethoxyphenyl)-4,5-dimethoxyphenyl]ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 29799-22-2
1,1'-(6,6'-dihydroxy-5,5'-dimethoxy-(1,1'-biphenyl)-3,3'-diyl)-bis-(ethan-1-one)

: 74-88-4
methyl iodide

: 55919-72-7
1,1'-(5,5',6,6'-tetramethoxy-1,1'-biphenyl-3,3'-diyl)diethanone

Guidance literature:: With potassium hydroxide; In ethanol; at 50 ℃; for 12h;
DOI:10.1016/S0957-4166(03)00449-X

Reference yield: 80.0%

: 91471-08-8
3-methoxy-4-(tetrahydropyran-2-yloxy)benzaldehyde

: 55919-72-7
1,1'-(5,5',6,6'-tetramethoxy-1,1'-biphenyl-3,3'-diyl)diethanone

: (2E,2'E)-1,1'-(5,5',6,6'-tetramethoxy-[1,1'-biphenyl]-3,3'-diyl)bis(3-(4-hydroxy-3-methoxyphenyl)prop-2-en-1-one)

Guidance literature:: 3-methoxy-4-(tetrahydropyran-2-yloxy)benzaldehyde; 1,1'-(5,5',6,6'-tetramethoxy-1,1'-biphenyl-3,3'-diyl)diethanone; With potassium hydroxide; In methanol; water; at 0 - 20 ℃; for 15h; Inert atmosphere;

With toluene-4-sulfonic acid; In methanol; water; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.3390/molecules25112709