Technology Process of Methyl 2,2,3,3-tetramethoxypropanoate
There total 2 articles about Methyl 2,2,3,3-tetramethoxypropanoate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
zinc dibromide;
In
dichloromethane;
for 18h;
Ambient temperature;
- Guidance literature:
-
With
tert.-butyl lithium; oxygen;
Yield given. Multistep reaction. Yields of byproduct given;
1.) ether, -78 deg C, 20 min, 2.) ether, -78 deg C, 3 h -> room temperature;