N-hydroxy-1-methyl-2,6-diphenylpiperidin-4-imine

Base Information

Chemical Name:N-hydroxy-1-methyl-2,6-diphenylpiperidin-4-imine
CAS No.:27771-21-7
Molecular Formula:C₁₈H₂₀N₂O
Molecular Weight:280.37
Hs Code.:
Mol file:27771-21-7.mol

Synonyms:4-Piperidinone,1-methyl-2,6-diphenyl-, oxime, cis-; 4-Piperidone, 1-methyl-2,6-diphenyl-,oxime, cis- (8CI); NSC 132834

Suppliers and Price of N-hydroxy-1-methyl-2,6-diphenylpiperidin-4-imine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of N-hydroxy-1-methyl-2,6-diphenylpiperidin-4-imine

Chemical Property:

Vapor Pressure:2.2E-08mmHg at 25°C
Boiling Point:436.3°Cat760mmHg
Flash Point:217.7°C
Density:1.12g/cm³

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of N-hydroxy-1-methyl-2,6-diphenylpiperidin-4-imine

There total 4 articles about N-hydroxy-1-methyl-2,6-diphenylpiperidin-4-imine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 39653-65-1,5554-56-3
1-methyl-2,6-diphenyl-piperidin-4-one

: 13245-77-7,27771-21-7,64912-36-3,67667-99-6
1-methyl-2,6-diphenylpiperidin-4-one oxime

Guidance literature:: With hydroxylamine hydrochloride; sodium acetate; In ethanol; for 1.5h; Heating;
DOI:10.1016/j.ejmech.2006.02.005

Reference yield:

: 100-52-7
benzaldehyde

: 13245-77-7,27771-21-7,64912-36-3,67667-99-6
1-methyl-2,6-diphenylpiperidin-4-one oxime

Guidance literature:: Multi-step reaction with 3 steps

1: NH₄OAc; HCl / ethanol; diethyl ether

2: 91 percent / potassium carbonate / acetone / 3.5 h / 45 - 55 °C

3: 90 percent / NaOAc*3H₂O; NH₂OH*HCl / ethanol / 1.5 h / Heating

With hydrogenchloride; hydroxylamine hydrochloride; ammonium acetate; sodium acetate; potassium carbonate; In diethyl ether; ethanol; acetone; 1: Mannich reaction;
DOI:10.1016/j.ejmech.2006.02.005

Reference yield:

: 5554-55-2,54750-61-7
2,6-diphenyl-4-piperidone

: 13245-77-7,27771-21-7,64912-36-3,67667-99-6
1-methyl-2,6-diphenylpiperidin-4-one oxime

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / potassium carbonate / acetone / 3.5 h / 45 - 55 °C

2: 90 percent / NaOAc*3H₂O; NH₂OH*HCl / ethanol / 1.5 h / Heating

With hydroxylamine hydrochloride; sodium acetate; potassium carbonate; In ethanol; acetone;
DOI:10.1016/j.ejmech.2006.02.005