3-(4-Methylphenyl)sulfonyl-1,2,4,5-tetrahydro-3-benzazepine

Base Information

Chemical Name:3-(4-Methylphenyl)sulfonyl-1,2,4,5-tetrahydro-3-benzazepine
CAS No.:15299-53-3
Molecular Formula:C₁₇H₁₉NO₂S
Molecular Weight:301.409
Hs Code.:
NSC Number:92826
DSSTox Substance ID:DTXSID40293898
Wikidata:Q82032898
ChEMBL ID:CHEMBL1701308
Mol file:15299-53-3.mol

Synonyms:MLS002695149;15299-53-3;NSC92826;CHEMBL1701308;DTXSID40293898;HMS3087I22;NSC-92826;SMR001561061

Suppliers and Price of 3-(4-Methylphenyl)sulfonyl-1,2,4,5-tetrahydro-3-benzazepine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of 3-(4-Methylphenyl)sulfonyl-1,2,4,5-tetrahydro-3-benzazepine

Chemical Property:

Vapor Pressure:8.85E-09mmHg at 25°C
Boiling Point:463.7°C at 760 mmHg
Flash Point:234.3°C
Density:1.212g/cm³
XLogP3:3.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:301.11365002
Heavy Atom Count:21
Complexity:418

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC=C(C=C1)S(=O)(=O)N2CCC3=CC=CC=C3CC2

Technology Process of 3-(4-Methylphenyl)sulfonyl-1,2,4,5-tetrahydro-3-benzazepine

There total 3 articles about 3-(4-Methylphenyl)sulfonyl-1,2,4,5-tetrahydro-3-benzazepine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2184-00-1
2,4-Dioxo-2,3,4,5-tetrahydro-1H-3-benzazepin

: 15299-53-3
3-(toluene-4-sulfonyl)-2,3,4,5-tetrahydro-1H-benz[d]azepine

Guidance literature:: Multi-step reaction with 2 steps

1: dioxane; lithium alanate; diethyl ether

2: lithium alanate; dioxane; diethyl ether / Reaktion ueber zwei Stufen

With 1,4-dioxane; lithium aluminium tetrahydride; diethyl ether;
DOI:10.1021/jo50012a012

Reference yield:

: 7500-54-1
o-xylylenediamide

: 15299-53-3
3-(toluene-4-sulfonyl)-2,3,4,5-tetrahydro-1H-benz[d]azepine

Guidance literature:: Multi-step reaction with 3 steps

1: 295 °C / 30 Torr

2: dioxane; lithium alanate; diethyl ether

3: lithium alanate; dioxane; diethyl ether / Reaktion ueber zwei Stufen

With 1,4-dioxane; lithium aluminium tetrahydride; diethyl ether;
DOI:10.1021/jo50012a012