3-Chloro-2-methoxypropene

Base Information

• Chemical Name: 3-Chloro-2-methoxypropene
• CAS No.: 32730-64-6
• Molecular Formula: C4H7 Cl O
• Molecular Weight: 106.552
• Hs Code.: 2909199090
• European Community (EC) Number: 251-179-9
• DSSTox Substance ID: DTXSID90186403
• Nikkaji Number: J319.442F
• Mol file: 32730-64-6.mol

Synonyms:3-Chloro-2-methoxypropene;32730-64-6;3-chloro-2-methoxyprop-1-ene;1-Propene,3-chloro-2-methoxy-;EINECS 251-179-9;1-Propene, 3-chloro-2-methoxy-;3-Chloro-2-methoxy-1-propene;SCHEMBL12655279;DTXSID90186403;AKOS006326426;FT-0774901

Chemical Property of 3-Chloro-2-methoxypropene

Chemical Property:

• Vapor Pressure: 26.6mmHg at 25°C
• Boiling Point: 111.6°Cat760mmHg
• Flash Point: 31.5°C
• PSA: 9.23000
• Density: 0.993g/cm³
• LogP: 1.38530
• XLogP3: 1.2
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 2
• Exact Mass: 106.0185425
• Heavy Atom Count: 6
• Complexity: 51.5

Purity/Quality:

99% ^*data from raw suppliers

3-CHLORO-2-METHOXYPROPENE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: COC(=C)CCl

Technology Process of 3-Chloro-2-methoxypropene

There total 3 articles about 3-Chloro-2-methoxypropene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-Methoxypropene (116-11-0) → 3-chloroprop-1-en-2-yl methyl ether (32730-64-6)

Guidance literature:

With N-chloro-succinimide; In tetrachloromethane; Heating;

DOI:10.1021/jo00969a021

Reference yield:

α-chloroacetone dimethyl acetal (32730-70-4) → 3-chloroprop-1-en-2-yl methyl ether (32730-64-6)

Guidance literature:

With quinolinium dihydrogenphosphate; at 270 ℃;

Reference yield:

α-chloroacetone dimethyl acetal (32730-70-4) → 3-chloroprop-1-en-2-yl methyl ether (32730-64-6)

Guidance literature:

at 270 ℃;

upstream raw materials:

α-chloroacetone dimethyl acetal

2-Methoxypropene

Downstream raw materials:

5-(2-methoxy-allyl)-5-phenyl-barbituric acid

Refernces

• 1、 -. "A NOVEL PROCESS FOR THE PREPARATION OF ANTHRANILIC DIAMIDES". Page/Page column 51; 66. . Retrieved 2019/12/15.