benzyl alcohol xylopyranosyl-(1-6)-glucopyranoside

Base Information

• Chemical Name: benzyl alcohol xylopyranosyl-(1-6)-glucopyranoside
• CAS No.: 130622-31-0
• Molecular Formula: C18H26 O10
• Molecular Weight: 402.398
• ChEMBL ID: CHEMBL1371061
• Wikidata: Q105309488
• Mol file: 130622-31-0.mol

Synonyms:Benzylalcohol b-D-xylopyranosyl(1®6)-b-D-glucopyranoside; Benzyl b-primeveroside

Chemical Property of benzyl alcohol xylopyranosyl-(1-6)-glucopyranoside

Chemical Property:

• Vapor Pressure: 3.41E-18mmHg at 25°C
• Boiling Point: 657.7°Cat760mmHg
• Flash Point: 351.6°C
• PSA: 158.30000
• Density: 1.52g/cm³
• LogP: -2.53360
• XLogP3: -2.8
• Hydrogen Bond Donor Count: 6
• Hydrogen Bond Acceptor Count: 10
• Rotatable Bond Count: 6
• Exact Mass: 402.15259702
• Heavy Atom Count: 28
• Complexity: 473

Purity/Quality:

98%min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1C(C(C(C(O1)OCC2C(C(C(C(O2)OCC3=CC=CC=C3)O)O)O)O)O)O

Technology Process of benzyl alcohol xylopyranosyl-(1-6)-glucopyranoside

There total 12 articles about benzyl alcohol xylopyranosyl-(1-6)-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

benzyl 2,3,4-tri-O-acetyl-β-D-glucopyranoside (29868-41-5) + (2S,3R,4S,5R)-2-(phenylthio)tetrahydro-2H-pyran-3,4,5-triyl triacetate (52544-91-9,52544-92-0,62774-34-9,98461-49-5,107961-02-4,107961-33-1,110221-83-5) → benzyl β-D-xylopyranosyl-(1->4)-β-D-glucopyranoside + benzyl β-primeveroside (130622-31-0)

Guidance literature:

benzyl 2,3,4-tri-O-acetyl-β-D-glucopyranoside; (2S,3R,4S,5R)-2-(phenylthio)tetrahydro-2H-pyran-3,4,5-triyl triacetate; With N-iodo-succinimide; trifluorormethanesulfonic acid; In dichloromethane; at 0 ℃; for 3.5h;

With potassium carbonate; In methanol; at 20 ℃; for 12h;

DOI:10.1248/cpb.53.1058

Reference yield: 51.0%

benzyl alcohol (100-51-6,185532-71-2) + p-nitrophenyl 6-O-β-D-xylopyranosyl-β-D-glucopyranoside → benzyl β-primeveroside (130622-31-0)

Guidance literature:

With sodium acetate buffer; Penicillium multicolor IAM7153 β-primeverosidase; In water; at 40 ℃; for 3.5h; pH=5.5;

DOI:10.1080/07328300500439413

Reference yield:

C60H50O16 (192827-12-6) → benzyl β-primeveroside (130622-31-0)

Guidance literature:

With sodium methylate; In methanol; for 15h; Ambient temperature;

DOI:10.1021/jf960852b

upstream raw materials:

C₆₀H₅₀O₁₆

benzyl 2,3,4-tri-O-acetyl-β-D-glucopyranoside

(2S,3R,4S,5R)-2-(phenylthio)tetrahydro-2H-pyran-3,4,5-triyl triacetate

benzyl alcohol

Downstream raw materials:

1-O-β-D-xylopyranosyl-(1,6)-β-D-glucopyranoside

benzyl alcohol