[2,2,4-Trimethyl-1-(3-phenylprop-2-enoyl)quinolin-6-yl] 3-phenylprop-2-enoate

Base Information

• Chemical Name: [2,2,4-Trimethyl-1-(3-phenylprop-2-enoyl)quinolin-6-yl] 3-phenylprop-2-enoate
• CAS No.: 4599-58-0
• Molecular Formula: C30H27NO3
• Molecular Weight: 222.238
• DSSTox Substance ID: DTXSID90389533

Synonyms:4599-58-0;DTXSID90389533;[2,2,4-trimethyl-1-(3-phenylprop-2-enoyl)quinolin-6-yl] 3-phenylprop-2-enoate

Chemical Property of [2,2,4-Trimethyl-1-(3-phenylprop-2-enoyl)quinolin-6-yl] 3-phenylprop-2-enoate

Chemical Property:

• Vapor Pressure: 4.94E-15mmHg at 25°C
• Boiling Point: 614.5°C at 760 mmHg
• Flash Point: 325.4°C
• Density: 1.171g/cm³
• XLogP3: 6.1
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 6
• Exact Mass: 449.19909372
• Heavy Atom Count: 34
• Complexity: 811

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1=CC(N(C2=C1C=C(C=C2)OC(=O)C=CC3=CC=CC=C3)C(=O)C=CC4=CC=CC=C4)(C)C

Technology Process of [2,2,4-Trimethyl-1-(3-phenylprop-2-enoyl)quinolin-6-yl] 3-phenylprop-2-enoate

There total 2 articles about [2,2,4-Trimethyl-1-(3-phenylprop-2-enoyl)quinolin-6-yl] 3-phenylprop-2-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5,7,4'-trihydroxy-3'-methoxyflavone-4'-O-α-L-rhamnopyranosyl-(1→4)-O-α-L-arabino-pyranosyl-(1→3)-O-β-D-galactopyranoside + methyl iodide (74-88-4) → (3R,4R,5S,6S)-3,4,5-trimethoxy-6-methyltetrahydro-2H-pyran-2-ol (14187-51-0) + 2,3,6-tri-O-methyl-D-galactopyranose (4599-58-0) + 2,3-di-O-methyl-L-arabinose + 2-(3,4-dimethoxyphenyl)-5,7-dimethoxy-4H-chromen-4-one (855-97-0)

Guidance literature:

With silver(l) oxide; In N,N-dimethyl-formamide; for 24h; Reflux;

DOI:10.14233/ajchem.2013.13533

Reference yield:

C66H116O24 (41670-15-9,57526-62-2) → 2,3,4,6-tetra-O-methyl-D-glucopyranose (1139-97-5,1139-98-6,1851-12-3,3353-52-4,6163-35-5,14184-49-7,19146-17-9,22248-57-3,34361-56-3,34361-57-4,57793-53-0,7506-68-5) + O3,O4,O6-trimethyl-D-glucose (13554-85-3,14184-50-0,35775-27-0,35775-28-1,38184-02-0,52194-59-9,52194-60-2) + 2,3,6-tri-O-methyl-D-galactopyranose (4599-58-0) + Neotigogenin (77-60-1,126-18-1,126-19-2,428-41-1,470-00-8,470-01-9,470-03-1,546-41-8,6788-40-5,7050-46-6,16653-88-6,19043-98-2,20460-38-2,31356-48-6,36027-61-9,36136-35-3,75172-34-8,78964-18-8,82597-74-8,107380-02-9,119677-72-4)

Guidance literature:

With sulfuric acid; In methanol; water; for 6h; Heating;

DOI:10.1007/BF00568374

upstream raw materials:

C₆₆H₁₁₆O₂₄

methyl iodide

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