4-{[(E)-(2-chlorophenyl)methylidene]amino}phenol

Base Information

• Chemical Name: 4-{[(E)-(2-chlorophenyl)methylidene]amino}phenol
• CAS No.: 6272-16-8
• Molecular Formula: C13H10 Cl N O
• Molecular Weight: 231.681

Synonyms:Phenol,p-[(o-chlorobenzylidene)amino]- (7CI,8CI); 4-(o-Chlorobenzylideneamino)phenol;NSC 37084

Chemical Property of 4-{[(E)-(2-chlorophenyl)methylidene]amino}phenol

Chemical Property:

• Vapor Pressure: 2.91E-07mmHg at 25°C
• Boiling Point: 408.7°Cat760mmHg
• Flash Point: 200.9°C
• Density: 1.18g/cm³

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-{[(E)-(2-chlorophenyl)methylidene]amino}phenol

There total 3 articles about 4-{[(E)-(2-chlorophenyl)methylidene]amino}phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

4-amino-phenol (123-30-8) + 2-chloro-benzaldehyde (89-98-5) → 4-{[(2-chlorophenyl)methylene]amino}phenol (6272-16-8)

Guidance literature:

With piperidine; In ethanol; Heating;

DOI:10.1080/10426509908031613

Reference yield:

4-nitro-phenol (100-02-7,78813-13-5,89830-32-0) → 4-{[(2-chlorophenyl)methylene]amino}phenol (6272-16-8)

Guidance literature:

With sulfuric acid; iron; beim Erwaermen der mit Magnesiumoxid versetzen Reaktionsloesung mit 2-Chlor-benzaldehyd;

Reference yield:

→ 4-{[(2-chlorophenyl)methylene]amino}phenol (6272-16-8)

Guidance literature:

4-Hydroxy-anilin, 2-Chlor-benzaldehyd;

upstream raw materials:

4-nitro-phenol

4-amino-phenol

2-chloro-benzaldehyde

Downstream raw materials:

1-(2-chlorobenzyl)-2,7-dioxo-1-azaspiro[3.5]nona-5,8-diene-3-carbonitrile

N-(2-chlorobenzyl)-2-cyano-N-(4-hydroxyphenyl)acetamide

C₁₃H₁₂ClNO

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