4-Butyl-1-(p-(methylsulfonyl)phenyl)-2-phenyl-3,5-pyrazolidinedione

Base Information

Chemical Name:4-Butyl-1-(p-(methylsulfonyl)phenyl)-2-phenyl-3,5-pyrazolidinedione
CAS No.:2019-05-8
Molecular Formula:C₂₀H₂₂N₂O₄S
Molecular Weight:386.472
Hs Code.:
DSSTox Substance ID:DTXSID20942251
Nikkaji Number:J1.855.311B

Synonyms:2019-05-8;G 34764;BRN 0901049;DTXSID20942251;4-Butyl-1-(p-(methylsulfonyl)phenyl)-2-phenyl-3,5-pyrazolidinedione;1-Phenyl-2-(p-methylsulfon-phenyl)-3,5-dioxo-4-n-butylpyrazolidin [German];3,5-Pyrazolidinedione, 4-butyl-1-(p-(methylsulfonyl)phenyl)-2-phenyl-;5-24-05-00406 (Beilstein Handbook Reference);1-Phenyl-2-(p-methylsulfon-phenyl)-3,5-dioxo-4-n-butylpyrazolidin;4-Butyl-1-[4-(methanesulfonyl)phenyl]-2-phenylpyrazolidine-3,5-dione

Suppliers and Price of 4-Butyl-1-(p-(methylsulfonyl)phenyl)-2-phenyl-3,5-pyrazolidinedione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 4-Butyl-1-(p-(methylsulfonyl)phenyl)-2-phenyl-3,5-pyrazolidinedione

Chemical Property:

Vapor Pressure:1.68E-12mmHg at 25°C
Boiling Point:558.4°C at 760 mmHg
Flash Point:291.5°C
Density:1.268g/cm³
XLogP3:2.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:6
Exact Mass:386.13002836
Heavy Atom Count:27
Complexity:643

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCCC1C(=O)N(N(C1=O)C2=CC=C(C=C2)S(=O)(=O)C)C3=CC=CC=C3

Technology Process of 4-Butyl-1-(p-(methylsulfonyl)phenyl)-2-phenyl-3,5-pyrazolidinedione

There total 6 articles about 4-Butyl-1-(p-(methylsulfonyl)phenyl)-2-phenyl-3,5-pyrazolidinedione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 521972-81-6
4-methylsulfonylhydrazobenzene

: 17999-54-1
2-n-butylmalonyl dichloride

: 2019-05-8
4-n-butyl-1-(4-methylsulfonylphenyl)-2-phenyl-3,5-dioxopyrazolidine

Guidance literature:: In pyridine; benzene; for 4h; Heating;
DOI:10.1002/jhet.5570390631

Reference yield:

: 29454-39-5
4-methylthioazobenzene

: 2019-05-8
4-n-butyl-1-(4-methylsulfonylphenyl)-2-phenyl-3,5-dioxopyrazolidine

Guidance literature:: Multi-step reaction with 3 steps

1: potassium peroxymonosulfate / methanol; H₂O / 16 h / 25 °C

2: 75 percent / aq. ammonium chloride; zinc dust / acetone; methanol

3: 42 percent / pyridine; benzene / 4 h / Heating

With Oxone; ammonium chloride; zinc; In pyridine; methanol; water; acetone; benzene;
DOI:10.1002/jhet.5570390631

Reference yield:

: 586-96-9
Nitrosobenzene

: 2019-05-8
4-n-butyl-1-(4-methylsulfonylphenyl)-2-phenyl-3,5-dioxopyrazolidine

Guidance literature:: Multi-step reaction with 4 steps

1: 75 percent / glacial acetic acid / 0.33 h / 100 °C

2: potassium peroxymonosulfate / methanol; H₂O / 16 h / 25 °C

3: 75 percent / aq. ammonium chloride; zinc dust / acetone; methanol

4: 42 percent / pyridine; benzene / 4 h / Heating

With Oxone; ammonium chloride; acetic acid; zinc; In pyridine; methanol; water; acetone; benzene;
DOI:10.1002/jhet.5570390631