1-methyl-2,3-bis(acetoxymethyl)pyrrole

Base Information

Chemical Name:1-methyl-2,3-bis(acetoxymethyl)pyrrole
CAS No.:34082-83-2
Molecular Formula:C₁₁H₁₅NO₄
Molecular Weight:225.244
Hs Code.:2933990090
Mol file:34082-83-2.mol

Synonyms:1H-Pyrrole-2,3-dimethanol,1-methyl-, diacetate (ester) (9CI); Pyrrole-2,3-dimethanol, 1-methyl-,diacetate (ester) (8CI); 1-Methyl-2,3-bis-acetoxymethylpyrrole;1-Methyl-2,3-diacetoxymethylpyrrole; 2,3-Bisacetoxymethyl-1-methylpyrrole

Suppliers and Price of 1-methyl-2,3-bis(acetoxymethyl)pyrrole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 1 raw suppliers

Chemical Property of 1-methyl-2,3-bis(acetoxymethyl)pyrrole

Chemical Property:

Vapor Pressure:0.000799mmHg at 25°C
Boiling Point:305.9°Cat760mmHg
Flash Point:138.8°C
PSA：57.53000
Density:1.14g/cm³
LogP:1.15130

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1-methyl-2,3-bis(acetoxymethyl)pyrrole

There total 6 articles about 1-methyl-2,3-bis(acetoxymethyl)pyrrole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 161677-79-8
(2E,4E,6E)-diethyl 3,6-dicyano-2,7-dihydroxyocta-2,4,6-trienedioate

: 34082-83-2
2,3-bis(acetoxymethyl)-1-methylpyrrole

Guidance literature:: Multi-step reaction with 5 steps

1: 48 percent / ethyl acetate; H₂O; ethanol / 4 h / Heating

2: 98 percent / aq. NaOH / 6.5 h / 135 °C

3: 94 percent / trimethylsilyl chloride / 24 h / 25 °C

4: 100 percent / LiAlH₄ / diethyl ether / 1.5 h / Heating

5: triethylamine, 4-(dimethylamino)pyridine / CDCl₃ / 1 h

With dmap; sodium hydroxide; lithium aluminium tetrahydride; chloro-trimethyl-silane; triethylamine; In diethyl ether; chloroform-d1; ethanol; water; ethyl acetate;
DOI:10.1021/ja00062a002

Reference yield:

: 25472-58-6
Dimethyl 1-methyl-1H-pyrrole-2,3-dicarboxylate

: 34082-83-2
2,3-bis(acetoxymethyl)-1-methylpyrrole

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / LiAlH₄ / diethyl ether / 1.5 h / Heating

2: triethylamine, 4-(dimethylamino)pyridine / CDCl₃ / 1 h

With dmap; lithium aluminium tetrahydride; triethylamine; In diethyl ether; chloroform-d1;
DOI:10.1021/ja00062a002

Reference yield:

: 7164-21-8
2-carbethoxy-3-cyano-1-methylpyrrole

: 34082-83-2
2,3-bis(acetoxymethyl)-1-methylpyrrole

Guidance literature:: Multi-step reaction with 4 steps

1: 98 percent / aq. NaOH / 6.5 h / 135 °C

2: 94 percent / trimethylsilyl chloride / 24 h / 25 °C

3: 100 percent / LiAlH₄ / diethyl ether / 1.5 h / Heating

4: triethylamine, 4-(dimethylamino)pyridine / CDCl₃ / 1 h

With dmap; sodium hydroxide; lithium aluminium tetrahydride; chloro-trimethyl-silane; triethylamine; In diethyl ether; chloroform-d1;
DOI:10.1021/ja00062a002