methyl butoxyacetate

Base Information

• Chemical Name: methyl butoxyacetate
• CAS No.: 10228-54-3
• Molecular Formula: C7H14 O3
• Molecular Weight: 146.186
• Mol file: 10228-54-3.mol

Synonyms:Aceticacid, butoxy-, methyl ester (6CI,7CI,8CI,9CI); Butoxyacetic acid methyl ester;Methyl butoxyacetate; NSC 294108

Chemical Property of methyl butoxyacetate

Chemical Property:

• Vapor Pressure: 0.578mmHg at 25°C
• Boiling Point: 189.2°C at 760 mmHg
• Flash Point: 61.3°C
• Density: 0.949g/cm³

Purity/Quality:

98%min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of methyl butoxyacetate

There total 6 articles about methyl butoxyacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

methyl diazoacetate (6832-16-2) + butan-1-ol (71-36-3) → Methyl butoxyacetate (10228-54-3)

Guidance literature:

With Rh(III)-Mont K 10 clay; at 60 ℃; for 12h;

DOI:10.1039/a905028k

Reference yield:

bromoacetic acid methyl ester (96-32-2) + butan-1-ol (71-36-3) → Methyl butoxyacetate (10228-54-3)

Guidance literature:

butan-1-ol; With sodium; Cooling with ice; Reflux;

bromoacetic acid methyl ester; at 20 - 50 ℃;

Reference yield:

(Tetrahydro-furan-2-yloxy)-acetic acid methyl ester → Methyl butoxyacetate (10228-54-3)

Guidance literature:

With hydrogen; platinum(IV) oxide; at 180 - 190 ℃;

DOI:10.1007/BF00755264

upstream raw materials:

methyl diazoacetate

butan-1-ol

dibutyl ether

methanol

Downstream raw materials:

2-Butoxyethanol

butoxy-acetic acid cyclohexylamide

Refernces

• 1、 -. "VANCOMYCIN DERIVATIVE, AND PREPARATION METHOD AND APPLICATION THEREOF". Paragraph 0220; 0222-0223. . Retrieved 2016/08/17.
• 2、 Phukan, Prodeep,Mohan, Jakkam Madan,Sudalai, Arumugam. "Reaction of methyl diazoacetate with aldehydes, amines, thiols, alcohols and acids over transition metal-exchanged clays". . p. 3685 - 3689. Retrieved 2007/10/03.