4-Phenyl-1h-2,3-benzoxazine

Base Information

Chemical Name:4-Phenyl-1h-2,3-benzoxazine
CAS No.:17799-96-1
Molecular Formula:C14H11NO
Molecular Weight:209.247
Hs Code.:
NSC Number:111349
DSSTox Substance ID:DTXSID30296772
Nikkaji Number:J1.585.156B
Wikidata:Q82037525
ChEMBL ID:CHEMBL2272294

Synonyms:4-phenyl-1h-2,3-benzoxazine;17799-96-1;NSC111349;CHEMBL2272294;DTXSID30296772;NSC-111349

Suppliers and Price of 4-Phenyl-1h-2,3-benzoxazine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 4-Phenyl-1h-2,3-benzoxazine

Chemical Property:

Vapor Pressure:0.000161mmHg at 25°C
Boiling Point:341.2°C at 760 mmHg
Flash Point:130.6°C
Density:1.13g/cm³
XLogP3:3.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:209.084063974
Heavy Atom Count:16
Complexity:268

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1C2=CC=CC=C2C(=NO1)C3=CC=CC=C3

Technology Process of 4-Phenyl-1h-2,3-benzoxazine

There total 5 articles about 4-Phenyl-1h-2,3-benzoxazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: phenyl(2-(((propan-2-ylideneamino)oxy)methyl)phenyl) methanone

: 17799-96-1
4-phenyl-1H-benzo[d][1,2]oxazine

Guidance literature:: With hydrogenchloride; In water; at 60 ℃; for 1h;
DOI:10.1039/c8ob01400k

Reference yield: 65.0%

: 3532-25-0
N-benzyloxy benzamide

: 17799-96-1
4-phenyl-1H-benzo[d][1,2]oxazine

Guidance literature:: With 2-chloropyridine; trifluoromethylsulfonic anhydride; In dichloromethane; at 23 ℃; for 1h; Schlenk technique; Inert atmosphere;
DOI:10.1002/anie.202103806

Reference yield:

: phenyl-[2-(tetrahydro-pyran-2-yloxymethyl)-phenyl]-methanone

: 17799-96-1
4-phenyl-1H-benzo[d][1,2]oxazine

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / HONH₂*HCl; pyridine / methanol / Heating

2: 85 percent / diethyl azodicarboxylate; Ph₃P / 4-nitrophenol / tetrahydrofuran / 1 h / 20 °C

With pyridine; hydroxylamine hydrochloride; triphenylphosphine; diethylazodicarboxylate; 4-nitro-phenol; In tetrahydrofuran; methanol; 2: Mitsunobu reaction;
DOI:10.1016/S0040-4039(01)01406-X