Technology Process of tunicamycin III
There total 9 articles about tunicamycin III which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 87 percent / p-toluenesulfonic acid
2: 93 percent / pyridine
3: 72 percent / SeO2 / acetic acid
4: 19 percent / silver carbonate, silver oxide, silver perchlorate / CH2Cl2 / in dark
5: methanolic sodium methoxide
With
pyridine; selenium(IV) oxide; sodium methylate; silver perchlorate; toluene-4-sulfonic acid; silver carbonate; silver(l) oxide;
In
dichloromethane; acetic acid;
DOI:10.1016/S0040-4039(01)81486-6
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 93 percent / pyridine
2: 72 percent / SeO2 / acetic acid
3: 19 percent / silver carbonate, silver oxide, silver perchlorate / CH2Cl2 / in dark
4: methanolic sodium methoxide
With
pyridine; selenium(IV) oxide; sodium methylate; silver perchlorate; silver carbonate; silver(l) oxide;
In
dichloromethane; acetic acid;
DOI:10.1016/S0040-4039(01)81486-6
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 19 percent / silver carbonate, silver oxide, silver perchlorate / CH2Cl2 / in dark
2: methanolic sodium methoxide
With
sodium methylate; silver perchlorate; silver carbonate; silver(l) oxide;
In
dichloromethane;
DOI:10.1016/S0040-4039(01)81486-6