ALLYL 2-ACETAMIDO-2-DEOXY-ALPHA-D-GLUCOPYRANOSIDE

Base Information

• Chemical Name: ALLYL 2-ACETAMIDO-2-DEOXY-ALPHA-D-GLUCOPYRANOSIDE
• CAS No.: 54400-75-8
• Molecular Formula: C11H19NO6
• Molecular Weight: 261.275
• Hs Code.: 2932999099
• Mol file: 54400-75-8.mol

Synonyms:α-D-Glucopyranoside, 2-propenyl2-(acetylamino)-2-deoxy- (9CI);Allyl 2-acetamido-2-deoxy-α-D-glucopyranoside;Prop-2-en-1-yl 2-(acetylamino)-2-deoxyhexopyranoside;

Chemical Property of ALLYL 2-ACETAMIDO-2-DEOXY-ALPHA-D-GLUCOPYRANOSIDE

Chemical Property:

• Melting Point: 167-177°C
• Boiling Point: 541.7 °C at 760 mmHg
• Flash Point: 281.4 °C
• PSA: 108.25000
• Density: 1.3 g/cm³
• LogP: -1.47640
• Storage Temp.: 2-8°C

Purity/Quality:

98%Min ^*data from raw suppliers

Allyl 2-acetamido-2-deoxy-a-D-glucopyranoside ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of ALLYL 2-ACETAMIDO-2-DEOXY-ALPHA-D-GLUCOPYRANOSIDE

There total 46 articles about ALLYL 2-ACETAMIDO-2-DEOXY-ALPHA-D-GLUCOPYRANOSIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

allyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranoside (63064-48-2,116288-58-5,117299-90-8,126778-02-7,28738-44-5) → allyl 2-acetamido-2-deoxy-β-D-glucopyranoside (54400-75-8,64650-83-5,88903-97-3,116347-86-5,140849-88-3,144300-01-6,54400-77-0)

Guidance literature:

allyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranoside; With sodium methylate; In methanol; at 20 ℃;

In methanol; pH=7;

DOI:10.1055/s-0036-1591082

Reference yield: 100.0%

allyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-galactopyranoside (28738-44-5,63064-48-2,117299-90-8,126778-02-7,116288-58-5) → allyl-2-acetamido-2-deoxy-β-D-galactopyranoside (54400-75-8,54400-77-0,64650-83-5,88903-97-3,140849-88-3,144300-01-6,116347-86-5)

Guidance literature:

allyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-galactopyranoside; With sodium methylate; In methanol; at 20 ℃;

In methanol; pH=7;

DOI:10.1055/s-0036-1591082

Reference yield: 99.0%

N-Acetyl-D-glucosamine (7512-17-6,72-87-7,1136-42-1,1136-44-3,6082-29-7,6730-06-9,7772-94-3,10036-64-3,14131-60-3,14131-64-7,14131-68-1,14215-68-0,62057-49-2,62057-50-5,62057-51-6,62057-52-7,62057-53-8,62057-54-9,62057-55-0,62057-56-1,62075-50-7,62137-54-6,134451-97-1,134522-12-6,148347-16-4) + allyl alcohol (107-18-6) → allyl 2-acetamido-2-deoxy-α-D-glucopyranoside (54400-75-8)

Guidance literature:

With acetyl chloride; at 70 ℃; for 3h;

DOI:10.1039/b405344c

upstream raw materials:

allyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranoside

2-methyl-(3,4,6-tri-O-acetyl-1,2-dideoxy-α-D-glucopyranoso)[1,2-d]-2-oxazoline

N-Acetyl-D-glucosamine

allyl alcohol

Downstream raw materials:

allyl 2-deoxy-2-acetamido-4,6-O-benzylidene-β-D-glucopyranoside

allyl 2-acetamido-2-deoxy-4,6-O-(4-methoxybenzylidene)-β-D-glucopyranoside

allyl 2-acetamido-3,4-di-O-acetyl-2-deoxy-6-O-trityl-β-D-glucopyranoside

2-propenyl 2-acetamido-3,4,6-tri-O-benzyl-2-deoxy-β-D-glucopyranoside